Carbonimidic dichloride, (2,6-dichlorophenyl)-

Base Information

Chemical Name:Carbonimidic dichloride, (2,6-dichlorophenyl)-
CAS No.:21709-18-2
Molecular Formula:C7H3Cl4N
Molecular Weight:242.92
Hs Code.:
European Community (EC) Number:606-825-8
DSSTox Substance ID:DTXSID70485709
Nikkaji Number:J1.135.535H
Mol file:21709-18-2.mol

Synonyms:21709-18-2;Carbonimidic dichloride, (2,6-dichlorophenyl)-;1,1-dichloro-N-(2,6-dichlorophenyl)methanimine;N-(2,6-Dichlorophenyl)-carbonimidic Dichloride;(2,6-Dichlorophenyl)carbonimidic dichloride;starbld0005194;SCHEMBL25181750;DTXSID70485709;2,6-dichlorophenylcarbonimidic dichloride;dichloro-methylene-(2,6-dichloro-phenyl)-amine;1, 1-dichloro-N-(2, 6-dichlorophenyl)methanimine

Suppliers and Price of Carbonimidic dichloride, (2,6-dichlorophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-(2,6-Dichlorophenyl)-carbonimidicDichloride
5g
$ 1390.00

American Custom Chemicals Corporation
2,6 DICHLOROPHENYL CARBONIMIDIC DICHLORIDE 95.00%
5MG
$ 497.98

Total 9 raw suppliers

Chemical Property of Carbonimidic dichloride, (2,6-dichlorophenyl)-

Chemical Property:

Vapor Pressure:0.00219mmHg at 25°C
Boiling Point:298.9oC at 760 mmHg
Flash Point:134.6oC
PSA：12.36000
Density:1.53g/cm3
LogP:4.45850
Storage Temp.:Hygroscopic, -20°C Freezer, Under inert atmosphere
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:242.899010
Heavy Atom Count:12
Complexity:168

Purity/Quality:

> 95% ^*data from raw suppliers

N-(2,6-Dichlorophenyl)-carbonimidicDichloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)N=C(Cl)Cl)Cl
Uses N-(2,6-dichlorophenyl)-carbonimidic Dichloride is an impurity of clonidine (C587130). Chlonidine is α2-Adrenergic agonist. Antihypertensive; analgesic for neuropathic pain.

Technology Process of Carbonimidic dichloride, (2,6-dichlorophenyl)-

There total 5 articles about Carbonimidic dichloride, (2,6-dichlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 10113-35-6
N-(2,6-dichlorophenyl)-formamide

: 21709-18-2
N-(2,6-dichlorophenyl)-1,1-dichloromethanimine

Guidance literature:: With thionyl chloride; sulfuryl dichloride; at 60 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.06.008

Reference yield:

: 109384-39-6
N-(o-chlorophenyl)formohydroxamic acid

: 21709-18-2
N-(2,6-dichlorophenyl)-1,1-dichloromethanimine

Guidance literature:: With thionyl chloride; sulfuryl dichloride; Multistep reaction; 1.) ether, 0 deg C to 30 deg C, 1 h; 30 deg C, 2 h, 2.) 10 deg C to 30 deg C; 60 deg C, 16 h;
DOI:10.1055/s-1987-27847

Reference yield:

: 10468-16-3
2-chloro-N-hydroxybenzenamine

: 21709-18-2
N-(2,6-dichlorophenyl)-1,1-dichloromethanimine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / acetic anhydride / 16 h / 35 - 40 °C

2: 1.) SOCl₂, 2.) SOCL₂/SO₂Cl₂ / 1.) ether, 0 deg C to 30 deg C, 1 h; 30 deg C, 2 h, 2.) 10 deg C to 30 deg C; 60 deg C, 16 h

With thionyl chloride; sulfuryl dichloride; acetic anhydride;
DOI:10.1055/s-1987-27847