3,5-Diethyl-4-hydroxybenzaldehyde

Base Information

• Chemical Name: 3,5-Diethyl-4-hydroxybenzaldehyde
• CAS No.: 69574-07-8
• Molecular Formula: C11H14 O2
• Molecular Weight: 178.231
• Hs Code.: 2912499000
• European Community (EC) Number: 274-047-2
• DSSTox Substance ID: DTXSID10989630
• Nikkaji Number: J318.006I
• Wikidata: Q82978827
• Mol file: 69574-07-8.mol

Synonyms:3,5-Diethyl-4-hydroxybenzaldehyde;69574-07-8;EINECS 274-047-2;SCHEMBL1858187;DTXSID10989630;MLNOWFFHYALTKS-UHFFFAOYSA-N;2-(FMOC-AMINO)ETHYLBROMIDE;3,5-diethyl-4-hydroxy-benzaldehyde;CL9168;MFCD13152308;AKOS016002856;AM83268;DS-2358;CS-0152561;FT-0756832;EN300-2559897;A866806

Chemical Property of 3,5-Diethyl-4-hydroxybenzaldehyde

Chemical Property:

• Vapor Pressure: 0.0013mmHg at 25°C
• Boiling Point: 289.1°C at 760 mmHg
• Flash Point: 121.5°C
• PSA: 37.30000
• Density: 1.079g/cm³
• LogP: 2.32950
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 178.099379685
• Heavy Atom Count: 13
• Complexity: 154

Purity/Quality:

98%min ^*data from raw suppliers

3,5-Diethyl-4-hydroxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1=CC(=CC(=C1O)CC)C=O

Technology Process of 3,5-Diethyl-4-hydroxybenzaldehyde

There total 5 articles about 3,5-Diethyl-4-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

→ 3,5-diethyl-4-hydroxybenzaldehyde (69574-07-8)

Guidance literature:

Reference yield: 69.0%

Dichloromethyl methyl ether (4885-02-3) + 2,6-diethylphenol (1006-59-3) → 3,5-diethyl-4-hydroxybenzaldehyde (69574-07-8)

Guidance literature:

With titanium tetrachloride; at 20 ℃; for 3h;

DOI:10.1039/c1cc11681a

Reference yield:

hexamethylenetetramine (100-97-0) + 2,6-diethylphenol (1006-59-3) → 3,5-diethyl-4-hydroxybenzaldehyde (69574-07-8)

Guidance literature:

With acetic acid; at 120 ℃; for 3h; Heating / reflux;

upstream raw materials:

formaldehyd

2,6-diethylphenol

2,6-diethylaniline

hexamethylenetetramine

Downstream raw materials:

2,6-Diethyl-4-[2-(thien-2-yl)ethenyl]phenol

2,6-Diethyl-4-((E)-2-p-tolyl-vinyl)-phenol

4-[(E)-(3,5-dimethyl-4-nitrophenyl)vinyl]-2,6-diethylphenol

4-{(E)-[3,5-diethyl-4-(methoxymethoxy)]vinyl}-2,6-dimethylnitrobenzene

Refernces

• 1、 Ieda, Naoya,Nakagawa, Hidehiko,Horinouchi, Taeko,Peng, Tao,Yang, Dan,Tsumoto, Hiroki,Suzuki, Takayoshi,Fukuhara, Kiyoshi,Miyata, Naoki. "Peroxynitrite generation from a NO-releasing nitrobenzene derivative in response to photoirradiation". . p. 6449 - 6451. Retrieved 2011/06/27.
• 2、 -. "NOVEL THIOPHENE DERIVATIVES". Page/Page column 73. . Retrieved 2010/02/15.