1-Penten-3-ol, 4-methyl-1-phenyl-, (1E,3R)-

Base Information

Chemical Name:1-Penten-3-ol, 4-methyl-1-phenyl-, (1E,3R)-
CAS No.:220089-23-6
Molecular Formula:C12H16O
Molecular Weight:176.258
Hs Code.:
Mol file:220089-23-6.mol

Synonyms:

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Chemical Property of 1-Penten-3-ol, 4-methyl-1-phenyl-, (1E,3R)-

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Technology Process of 1-Penten-3-ol, 4-methyl-1-phenyl-, (1E,3R)-

There total 19 articles about 1-Penten-3-ol, 4-methyl-1-phenyl-, (1E,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 78-84-2
isobutyraldehyde

: 536-74-3
phenylacetylene

: 220089-23-6
trans-(R)-4-methyl-1-phenyl-1-penten-3-ol

Guidance literature:: phenylacetylene; With Diethylborane; In toluene; at 20 ℃; for 0.5h;

isobutyraldehyde; With (-)-MIB; diethylzinc; In hexane; toluene; at -78 - -10 ℃;
DOI:10.1021/ja0539239

Reference yield:

: 3160-32-5,5773-41-1,10596-48-2
(1E)-4-methyl-1-phenylpent-1-en-3-one

: 220089-23-6
trans-(R)-4-methyl-1-phenyl-1-penten-3-ol

: trans-(S)-4-methyl-1-phenyl-1-penten-3-ol

Guidance literature:: With (S,S)-RuCl₂(2,2'-bis(di-3,5-xylylphosphino)-1,1'-binaphthyl)(1,1-dianisyl-2-isopropyl-1,2-ethylenediamine); hydrogen; potassium carbonate; In isopropyl alcohol; at 28 - 30 ℃; for 20h; under 6080 Torr; Yield given; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja983257u

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 86983-95-1
(1E)-4-methyl-1-phenylpent-1-en-3-ol

: C₁₇H₂₆N₂O₂

: 220089-23-6
trans-(R)-4-methyl-1-phenyl-1-penten-3-ol

: trans-(S)-4-methyl-1-phenyl-1-penten-3-ol

Guidance literature:: With (S)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(diphenylphosphine); bis(η3-allyl-μ-chloropalladium(II)); 2,5-dichlorobenzenesulfonylhydrazide; In 1,4-dioxane; at 20 ℃; for 9h; under 760.051 Torr; enantioselective reaction;
DOI:10.1002/chem.201601747