5-Chloro-3-p-tolyl-[1,2,4]thiadiazole

Base Information

• Chemical Name: 5-Chloro-3-p-tolyl-[1,2,4]thiadiazole
• CAS No.: 221038-01-3
• Molecular Formula: C9H7ClN2S
• Molecular Weight: 210.687
• Hs Code.: 2934999090
• Mol file: 221038-01-3.mol

Synonyms:3-(p-tolyl)-5-chloro-1,2,4-thiadiazole;5-chloro-3-(4-methylphenyl)-1,2,4-thiadiazole;

Chemical Property of 5-Chloro-3-p-tolyl-[1,2,4]thiadiazole

Chemical Property:

• PSA: 54.02000
• LogP: 3.16690

Purity/Quality:

NLT 98% ^*data from raw suppliers

5-Chloro-3-p-tolyl-[1,2,4]thiadiazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 5-Chloro-3-p-tolyl-[1,2,4]thiadiazole

There total 3 articles about 5-Chloro-3-p-tolyl-[1,2,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

p-methylbenzamidine hydrochloride (6326-27-8) + chlorothio-trichloro-methane (594-42-3) → 5-chloro-3-p-tolyl-1,2,4-thiadiazole (221038-01-3)

Guidance literature:

With triethylamine; In dichloromethane; at -10 - 20 ℃; for 3h;

Reference yield: 85.0%

4-methylbenzimidamide hydrochloride + chlorothio-trichloro-methane (594-42-3) → 5-chloro-3-p-tolyl-1,2,4-thiadiazole (221038-01-3)

Guidance literature:

With triethylamine; In dichloromethane; at -10 - 20 ℃; for 3h;

Reference yield: 44.0%

trichloromethyl mercaptan (75-70-7) + p-methylbenzamidine hydrochloride (6326-27-8) → 5-chloro-3-p-tolyl-1,2,4-thiadiazole (221038-01-3)

Guidance literature:

With triethylamine; In chloroform;

upstream raw materials:

trichloromethyl mercaptan

p-methylbenzamidine hydrochloride

chlorothio-trichloro-methane

Downstream raw materials:

1-(3-p-tolyl-[1,2,4]thiadiazol-5-yl)-piperazine

1-benzo[1,3]dioxol-5-ylmethyl-4-(3-p-tolyl-[1,2,4]thiadiazol-5-yl)-piperazine

1-(2-methyl-benzyl)-4-(3-p-tolyl-[1,2,4]thiadiazol-5-yl)-piperazine

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