4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine

Base Information

• Chemical Name: 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine
• CAS No.: 30358-01-1
• Molecular Formula: C11H12 N4 O2
• Molecular Weight: 232.2386
• Mol file: 30358-01-1.mol

Synonyms:s-Triazine,2-anilino-4,6-dimethoxy- (6CI,8CI); 2-Anilino-4,6-dimethoxy-s-triazine

Chemical Property of 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine

Chemical Property:

• Vapor Pressure: 1.62E-06mmHg at 25°C
• Boiling Point: 397.2°C at 760 mmHg
• Flash Point: 194°C
• Density: 1.268g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine

There total 6 articles about 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-chloro-4,6-dimethoxy-1 ,3,5-triazine (3140-73-6) + aniline (62-53-3) → 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine (30358-01-1)

Guidance literature:

With 2-methylphenylzinc bromide; In acetonitrile; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1055/s-0030-1261220

Reference yield: 85.5%

methanol (67-56-1) + 2-phenylamino-4,6-dichloro-s-triazine (2272-40-4) → 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine (30358-01-1)

Guidance literature:

With lithium hydride; for 14h; cooling;

DOI:10.1007/s11172-006-0135-0

Reference yield: 56.0%

C18H16N4O3S → o-hydroxymethyl thiophenol (4521-31-7) + 4,6-dimethoxy-N-phenyl-1,3,5-triazin-2-amine (30358-01-1)

Guidance literature:

With sodium aluminum tetrahydride; In tetrahydrofuran; for 2.5h; Heating;

DOI:10.1016/j.tetlet.2007.11.096

upstream raw materials:

methanol

2-phenylamino-4,6-dichloro-s-triazine

aniline

2-hydroxyamino-4,6-dimethoxy-sym-triazine

Downstream raw materials:

2,4-di-n-butoxy-6-phenylamino-1,3,5-triazine