GaCl₂(4-methylpyridine)2(benzoato)*4-methylpyridine

Base Information

• Chemical Name: GaCl₂(4-methylpyridine)2(benzoato)*4-methylpyridine
• CAS No.: 1263600-02-7
• Molecular Formula: C₆H₇N*C₁₉H₁₉Cl₂GaN₂O₂
• Molecular Weight: 541.129
• Mol file: 1263600-02-7.mol

Synonyms:

Chemical Property of GaCl₂(4-methylpyridine)2(benzoato)*4-methylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of GaCl₂(4-methylpyridine)2(benzoato)*4-methylpyridine

There total 1 articles about GaCl₂(4-methylpyridine)2(benzoato)*4-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

picoline (108-89-4) + digallium tetrachloride (86884-85-7) + dibenzoyl peroxide (94-36-0) → GaCl2(4-methylpyridine)2(benzoato)*4-methylpyridine (1263600-02-7)

Guidance literature:

In further solvent(s); Ga-compd. and a 2:1 excess of benzoyl peroxide added to a Schlenk flask under N2, 4-methylpyridine slowly added via cannula with rapid stirring,stirred at room temp. for 48 h; filtered through a pad of Celite, hexane layered on the filtrate, kept for 72 h at room temp.;

DOI:10.1016/j.ica.2010.08.026

upstream raw materials:

picoline

digallium tetrachloride

dibenzoyl peroxide