Docosanedioic acid dimethyl ester

Base Information

• Chemical Name: Docosanedioic acid dimethyl ester
• CAS No.: 22399-98-0
• Molecular Formula: C24H46O4
• Molecular Weight: 398.627
• Hs Code.: 2917190090
• Mol file: 22399-98-0.mol

Synonyms:dimethyl docosanedicarboxylate;Docosandisaeure-dimethylester;Docosanedioic acid, dimethyl ester;Docosanedioic acid,dimethyl ester;

Chemical Property of Docosanedioic acid dimethyl ester

Chemical Property:

• PSA: 52.60000
• LogP: 7.13440

Purity/Quality:

98.5% ^*data from raw suppliers

DIMETHYL DOCOSANEDIOATE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Docosanedioic acid dimethyl ester

There total 3 articles about Docosanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

12-methoxy-12-oxododecanoic acid (3903-40-0) → methyl undecanoate (1731-86-8) + Methyl 10-undecenoate (111-81-9) + docosanedioic acid dimethyl ester (22399-98-0)

Guidance literature:

With potassium methanolate; In methanol; at 40 - 45 ℃; Yield given; electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm^-2; current consumption: 1.25 F mol^-1; cell voltage 40-70 V;

DOI:10.3891/acta.chem.scand.52-0672

Reference yield:

methanol (67-56-1) + cis-cyclododecene (1129-89-1) → methyl undecanoate (1731-86-8) + dodecanedioic acid dimethyl ester (1731-79-9) + docosanedioic acid dimethyl ester (22399-98-0) + cyclododecane (294-62-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1016/S0040-4020(01)91447-4

Reference yield:

cis-cyclododecene (1129-89-1) → methyl undecanoate (1731-86-8) + dodecanedioic acid dimethyl ester (1731-79-9) + docosanedioic acid dimethyl ester (22399-98-0) + cyclododecane (294-62-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1016/S0040-4020(01)91447-4

upstream raw materials:

methanol

cis-cyclododecene

12-methoxy-12-oxododecanoic acid

Downstream raw materials:

22-hydroxy-tetracosanoic acid methyl ester

22-hydroxy-tetracosanoic acid

22-hydroxydocosanoic acid

1,2-bis[p-(benzyliminomethylene)phenoxy]docosane