N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine

Base Information

Chemical Name:N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine
CAS No.:229007-08-3
Molecular Formula:C13H18N2O3
Molecular Weight:250.298
Hs Code.:
DSSTox Substance ID:DTXSID60436942
Nikkaji Number:J2.502.208D
Wikidata:Q82252291
Mol file:229007-08-3.mol

Synonyms:229007-08-3;N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine;SCHEMBL313713;DTXSID60436942;N-(4-Nitrobenzyl)-N-methyltetrahydro-4H-pyran-4-amine

Suppliers and Price of N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:250.13174244
Heavy Atom Count:18
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CC1=CC=C(C=C1)[N+](=O)[O-])C2CCOCC2

Technology Process of N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine

There total 6 articles about N-methyl-N-[(4-nitrophenyl)methyl]oxan-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 18600-42-5
4-nitrobenzylamine hydrochloride

: 229007-08-3
N-[(4-nitrophenyl)methyl]tetrahydro-N-methyl-2H-pyran-4-amine

Guidance literature:: Tetrahydro-4H-pyran-4-one; 4-nitrobenzylamine hydrochloride; With triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 0 - 20 ℃; for 6h;

formaldehyd; With sodium hydroxide; sodium tris(acetoxy)borohydride; more than 3 stages;

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 874888-66-1
4-[N-(tetrahydropyran-4-yl)aminomethyl]-nitrobenzene

: 229007-08-3
N-[(4-nitrophenyl)methyl]tetrahydro-N-methyl-2H-pyran-4-amine

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1021/jm9906264

Reference yield: 87.8%

: 392277-22-4
N-methyl-N-(tetrahydropyran-4-yl)amine hydrochloride

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 229007-08-3
N-[(4-nitrophenyl)methyl]tetrahydro-N-methyl-2H-pyran-4-amine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 3h; Temperature; Large scale;
DOI:10.1021/op010052o