Benzoic acid, 4-(bromomethyl)-, 2,2,2-trichloroethyl ester

Base Information

Chemical Name:Benzoic acid, 4-(bromomethyl)-, 2,2,2-trichloroethyl ester
CAS No.:233265-93-5
Molecular Formula:C10H8BrCl3O2
Molecular Weight:346.435
Hs Code.:
Mol file:233265-93-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-(bromomethyl)-, 2,2,2-trichloroethyl ester

Chemical Property:

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Technology Process of Benzoic acid, 4-(bromomethyl)-, 2,2,2-trichloroethyl ester

There total 3 articles about Benzoic acid, 4-(bromomethyl)-, 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.8%

: 233265-92-4
2,2,2-trichloroethyl p-methylbenzoate

: 233265-93-5
4-bromomethyl benzoic acid 2,2,2-trichloroethyl ester

Guidance literature:: With N-Bromosuccinimide; Perbenzoic acid; In benzene; for 1h; Heating;
DOI:10.1021/jm970091j

Reference yield:

: 115-20-8
1,1,1-trichloroethanol

: 876-07-3
4-(bromomethyl)benzoyl bromide

: 233265-93-5
4-bromomethyl benzoic acid 2,2,2-trichloroethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 233265-93-5
4-bromomethyl benzoic acid 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Et₃N / CHCl₃ / Heating

2: 76.8 percent / N-bromosuccinimide, benzoyl peroxide / benzene / 1 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; triethylamine; In chloroform; benzene;
DOI:10.1021/jm970091j