7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one

Base Information

Chemical Name:7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one
CAS No.:36519-17-2
Molecular Formula:C15H17 N5 O8
Molecular Weight:395.3242
Hs Code.:
Mol file:36519-17-2.mol

Synonyms:2',3',5'-Tri-O-acetyl-2-azainosine;NSC 158897

Suppliers and Price of 7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one

Chemical Property:

Vapor Pressure:1.05E-14mmHg at 25°C
Boiling Point:607.5°C at 760 mmHg
Flash Point:321.2°C
Density:1.71g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one

There total 4 articles about 7-(2,3,5-tri-O-acetylpentofuranosyl)-1,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 36519-16-1
7-((2R,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-3,7-dihydro-4H-imidazo[4,5-d][1,2,3]triazin-4-one

: 108-24-7
acetic anhydride

: 36519-17-2
7-(2,3,5,-tri-O-acetyl-β-D-ribofuranosyl)imidazo[4,5-d][1,2,3]triazin-4-one

Guidance literature:: In pyridine; at 60 ℃; for 24h;
DOI:10.1021/jo00125a009

Reference yield:

: 4656-86-4
2-azahypoxanthine

: 13035-61-5
1,2,3,5-tetraacetylribose

: 36519-17-2
7-(2,3,5,-tri-O-acetyl-β-D-ribofuranosyl)imidazo[4,5-d][1,2,3]triazin-4-one

: 1643356-24-4
C₁₅H₁₇N₅O₈

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; Overall yield = < 28 %;
DOI:10.1039/c4ob00705k

Reference yield:

: 2627-69-2
AICA riboside

: 36519-17-2
7-(2,3,5,-tri-O-acetyl-β-D-ribofuranosyl)imidazo[4,5-d][1,2,3]triazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; hydrogenchloride / water; ethanol / 2 h / -30 °C

2: pyridine / 16 h / 20 °C

With pyridine; hydrogenchloride; sodium nitrite; In ethanol; water;