tripropan-2-ylaluminum

Base Information

• Chemical Name: tripropan-2-ylaluminum
• CAS No.: 2397-67-3
• Molecular Formula: C9H21Al
• Molecular Weight: 156.247
• Mol file: 2397-67-3.mol

Synonyms:

Chemical Property of tripropan-2-ylaluminum

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tripropan-2-ylaluminum

There total 3 articles about tripropan-2-ylaluminum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diisopropylmercury (1071-39-2) → triisopropylaluminium (2397-67-3)

Guidance literature:

With aluminium; at 60 - 70 ℃; und auf 110-120grad;

DOI:10.1021/ja01215a027

Reference yield:

aluminium trichloride (7446-70-0) + isopropylmagnesium bromide (920-39-8) → triisopropylaluminium (2397-67-3)

Guidance literature:

In diethyl ether; toluene; i-PrMgBr in diethyl ether is added dropwise to well-stirred and refluxing toluene, suspn. is cooled to room temp., anhydrous AlCl3 is added, stirred at room temp. overnight; ppt. is centrifuged, vac. distn.;

DOI:10.1021/om00093a020

Reference yield:

→ triisopropylaluminium (2397-67-3)

Guidance literature:

Di-2-propylaluminiumfluorid 6, 2-Propyllithium;

upstream raw materials:

diisopropylmercury

aluminium trichloride

isopropylmagnesium bromide

Downstream raw materials:

dichloroisopropylphosphine

tri-n-propylaluminum

Difluor-isopropyl-boran

2-Isopropylnaphthalene

Refernces

• 1、 Russell, Glen A.,Ngoviwatchai, Preecha,Tashtoush, Hasan I.. "Electron-transfer processes. 43. Attack of alkyl radicals upon 1-alkenyl and 1-alkynyl derivatives of tin and mercury". . p. 696 - 702. Retrieved 2008/10/08.