1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

Base Information

Chemical Name:1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane
CAS No.:24559-01-1
Molecular Formula:C12H18N4
Molecular Weight:218.302
Hs Code.:
DSSTox Substance ID:DTXSID80349787
Nikkaji Number:J564.201I
Wikidata:Q82125255
ChEMBL ID:CHEMBL1353433
Mol file:24559-01-1.mol

Synonyms:24559-01-1;1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane;HMS2282L13;MLS000078459;1H-Pyrazole, 1,1'-(1,2-ethanediyl)bis[3,5-dimethyl-;CHEMBL1353433;SCHEMBL17489160;DTXSID80349787;STK545992;AKOS005474487;SMR000041933;1,1'-ethane-1,2-diylbis(3,5-dimethyl-1H-pyrazole)

Suppliers and Price of 1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:218.153146591
Heavy Atom Count:16
Complexity:209

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NN1CCN2C(=CC(=N2)C)C)C

Technology Process of 1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

There total 1 articles about 1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 67-51-6
3,5-dimethyl-1H-pyrazole

: 106-93-4
ethylene dibromide

3,5-Dimethyl-1-vinyl-1H-pyrazole: 15967-75-6
3,5-Dimethyl-1-vinyl-1H-pyrazole

: 24559-01-1
1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

: 67000-35-5
1-(2-bromoethyl)-3,5-dimethyl-1H-pyrazole

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; for 1h; Yields of byproduct given; Heating;
DOI:10.1016/S0968-0896(98)00273-9

Reference yield: 60.0%

: 1124-19-2
phenyltin trichloride

: 24559-01-1
1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

: [(1,2-bis(3,5-dimethylpyrazol-1-yl)ethane)(C₆H₅)SnCl₃]-H₂O

Guidance literature:: In not given; pptn. on addn. of excess ligand to Sn-compd. (in Et2O and/or petroleum ether, not specified) at room temp. with stirring; collection; elem. anal.;
DOI:10.1016/0022-328X(95)05445-U

Reference yield: 50.0%

: 90760-41-1
bis[dibromo(phenyl)stannyl]methane

: 24559-01-1
1,2-Bis(3,5-dimethylpyrazol-1-yl)ethane

: (bis(3,5-dimethylpyrazol-1-yl)ethane)bis(dibromophenylstannyl)methane

Guidance literature:: In dichloromethane; a soln. of Sn compd. added to a soln. of ligand (1 or 2 equiv.), stirredfor 2 h at room temp.; ppt. filtered, washed (cold ether), recrystd. (CH2Cl2-hexane); elem. anal.;
DOI:10.1016/S0277-5387(02)00863-X