(2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER

Base Information

Chemical Name:(2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER
CAS No.:24654-09-9
Molecular Formula:C11H9ClO2
Molecular Weight:208.644
Hs Code.:2916399090
Mol file:24654-09-9.mol

Synonyms:2-Chlorphenyl-propinsaeureethylester;ethyl 2-chlorophenylpropiolate;2-Chlor-phenylpropiolsaeure-ethylester;o-Chlor-phenyl-propiolsaeureethylester;

Suppliers and Price of (2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(2-CHLORO-PHENYL)PROPYNOIC ACID ETHYL ESTER 95.00%
5MG
$ 504.17

Total 3 raw suppliers

Chemical Property of (2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER

Chemical Property:

Vapor Pressure:0.00109mmHg at 25°C
Boiling Point:300.9oC at 760 mmHg
Flash Point:125oC
PSA：26.30000
Density:1.22g/cm3
LogP:2.25460

Purity/Quality:

95% ^*data from raw suppliers

(2-CHLORO-PHENYL)PROPYNOIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER

There total 10 articles about (2-CHLORO-PHENYL)-PROPYNOIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1170694-25-3
C₁₁H₁₀BrClO₂

: 24654-09-9
ethyl 3-(2-chlorophenyl)prop-2-ynoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; at 60 - 80 ℃; for 22h;
DOI:10.1016/j.cclet.2012.05.015

Reference yield: 79.0%

: 3-(2-Chloro-phenyl)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-propionic acid ethyl ester

: 24654-09-9
ethyl 3-(2-chlorophenyl)prop-2-ynoate

Guidance literature:: at 250 ℃; for 3h; under 0.1 Torr;

Reference yield: 78.0%

: 615-41-8
2-iodochlorobenzene

: 623-47-2
propynoic acid ethyl ester

: 24654-09-9
ethyl 3-(2-chlorophenyl)prop-2-ynoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; In 1,2-dimethoxyethane; at 40 ℃; for 13h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.202000823