N,N-Diethyl-3-fluorobenzenamine

Base Information

Chemical Name:N,N-Diethyl-3-fluorobenzenamine
CAS No.:2524-69-8
Molecular Formula:C10H14FN
Molecular Weight:167.226
Hs Code.:
DSSTox Substance ID:DTXSID601304966
Mol file:2524-69-8.mol

Synonyms:N,N-Diethyl-3-fluorobenzenamine;2524-69-8;SCHEMBL3425607;DTXSID601304966

Suppliers and Price of N,N-Diethyl-3-fluorobenzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N-Diethyl-3-fluorobenzenamine

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:167.111027613
Heavy Atom Count:12
Complexity:123

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C1=CC(=CC=C1)F

Technology Process of N,N-Diethyl-3-fluorobenzenamine

There total 8 articles about N,N-Diethyl-3-fluorobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1073-06-9
3-fluorobromobenzene

: 109-89-7
diethylamine

: 2524-69-8
m-fluoro-NN-diethylaniline

Guidance literature:: With copper(l) iodide; 2-(N,N-dimethylamino)ethanol; tripotassium phosphate "n" hydrate; copper; at 80 ℃; for 72h;

Reference yield:

: 109-89-7
diethylamine

: 460-00-4
1-Bromo-4-fluorobenzene

: 2524-69-8
m-fluoro-NN-diethylaniline

: 347-39-7
N,N-diethyl-4-methoxyaniline

Guidance literature:: With sodium t-butanolate; PdNaY; In toluene; at 135 ℃; for 20h; Title compound not separated from byproducts;
DOI:10.1016/S0022-328X(99)00518-5

Reference yield:

: 462-06-6
fluorobenzene

: 109-89-7
diethylamine

: 2524-69-8
m-fluoro-NN-diethylaniline

: 347-39-7
N,N-diethyl-4-methoxyaniline

Guidance literature:: palladium on activated charcoal; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) irradiation, 20-25 deg C, 24 h, 2.) toluene, reflux, 5 h;