Methyl 4,4-dimethoxy-2-methylbutanoate

Base Information

Chemical Name:Methyl 4,4-dimethoxy-2-methylbutanoate
CAS No.:25252-24-8
Molecular Formula:C8H16O4
Molecular Weight:176.21000
Hs Code.:2918990090
DSSTox Substance ID:DTXSID80510415
Nikkaji Number:J109.505F
Mol file:25252-24-8.mol

Synonyms:Methyl 4,4-dimethoxy-2-methylbutanoate;25252-24-8;DTXSID80510415

Suppliers and Price of Methyl 4,4-dimethoxy-2-methylbutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Methyl 4,4-dimethoxy-2-methylbutanoate

Chemical Property:

PSA：44.76000
LogP:0.80450
XLogP3:0.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:176.10485899
Heavy Atom Count:12
Complexity:131

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CC(OC)OC)C(=O)OC

Technology Process of Methyl 4,4-dimethoxy-2-methylbutanoate

There total 8 articles about Methyl 4,4-dimethoxy-2-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 130450-06-5
2-(2,2-Dimethoxy-ethyl)-2-methyl-malonic acid dimethyl ester

: 25252-24-8
3-methoxycarbonylbutyraldehyde dimethylacetal

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; Heating;
DOI:10.1055/s-1990-26929

Reference yield: 65.0%

: 67-56-1
methanol

: 6947-94-0
2-methyl-3-furancarboxylic acid

: 25252-24-8
3-methoxycarbonylbutyraldehyde dimethylacetal

Guidance literature:: With ammonium bromide; triethylamine; at 18 - 20 ℃; electrolysis: constant current = 2.5 A (current density = 62.5 mA/cm²), initial voltage = 14 V, final voltage = 40 V, amount of electricity passed = 8 F/mol;
DOI:10.1021/jo00140a051

Reference yield:

: 16507-03-2
2-methyl-4-nitro-butyric acid methyl ester

: 124-41-4
sodium methylate

: 25252-24-8
3-methoxycarbonylbutyraldehyde dimethylacetal

Guidance literature:: 2-methyl-4-nitro-butyric acid methyl ester; sodium methylate; In methanol; at 0 ℃; for 0.5h;

With sulfuric acid; In methanol; at 0 ℃; for 0.5h;
DOI:10.1021/acs.orglett.5b00437