1-Amino-1-deoxy-beta-D-galactose

Base Information

• Chemical Name: 1-Amino-1-deoxy-beta-D-galactose
• CAS No.: 6318-23-6
• Molecular Formula: C6H13 N O5
• Molecular Weight: 179.173
• Hs Code.: 2932999099
• European Community (EC) Number: 616-151-6
• NSC Number: 25270
• ChEMBL ID: CHEMBL359241
• Mol file: 6318-23-6.mol

Synonyms:mannosylamine

Chemical Property of 1-Amino-1-deoxy-beta-D-galactose

Chemical Property:

• Melting Point: 128-133°C
• Boiling Point: 416.4±45.0 °C(Predicted)
• PKA: 13.19±0.70(Predicted)
• PSA: 116.17000
• Density: 1.563±0.06 g/cm3(Predicted)
• LogP: -2.55470
• Storage Temp.: -20°C Freezer
• Solubility.: Methanol, Water
• XLogP3: -2.8
• Hydrogen Bond Donor Count: 5
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 179.07937252
• Heavy Atom Count: 12
• Complexity: 155

Purity/Quality:

98%, ^*data from raw suppliers

β-D-Galactopyranosylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C1C(C(C(C(O1)N)O)O)O)O
• Uses: β-D-Galactopyranosylamine (cas# 6318-23-6) is a compound useful in organic synthesis.

Technology Process of 1-Amino-1-deoxy-beta-D-galactose

There total 11 articles about 1-Amino-1-deoxy-beta-D-galactose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

D-Galactose (10257-28-0) → 1-amino-1-deoxy-β-D-galactose (6318-23-6,50444-86-5)

Guidance literature:

With ammonium hydroxide; ammonium bicarbonate; at 42 ℃; for 36h;

DOI:10.1016/0008-6215(94)00275-K

Reference yield: 100.0%

(2R,3R,4S,5R,6R)-2-Amino-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; compound with carbamic acid → 1-amino-1-deoxy-β-D-galactose (6318-23-6,50444-86-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In methanol; water; isopropyl alcohol;

DOI:10.1023/A:1015428720733

Reference yield: 76.0%

D-Galactose (59-23-4) → 1-amino-1-deoxy-β-D-galactose (6318-23-6,50444-86-5)

Guidance literature:

With ammonia; In methanol; at 50 ℃; for 8h;

DOI:10.1002/zaac.201500224

upstream raw materials:

D-Galactose

1-amido-1-deoxygalactopyranose

methanol

D-Galactose

Downstream raw materials:

N-bromoacetyl-β-D-galactopyranosylamine

(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-N-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-succinamic acid pentafluorophenyl ester

N¹-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)succinamic acid

(1,2-dideoxy-β-D-galactopyranoso)[1,2-d]-1,3-oxazolidine-2-thione

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