Phenol, 2-ethoxy-5-methyl-

Base Information

• Chemical Name: Phenol, 2-ethoxy-5-methyl-
• CAS No.: 2563-04-4
• Molecular Formula: C₉H₁₂O₂
• Molecular Weight: 152.193
• Hs Code.: 2909500090
• Mol file: 2563-04-4.mol

Synonyms:2-Aethoxy-5-methyl-phenol;2-ethoxy-5-methyl-phenol;1-Ethoxy-2-hydroxy-4-methyl-benzol;3-Oxy-4-aethoxy-1-methyl-benzol;

Chemical Property of Phenol, 2-ethoxy-5-methyl-

Chemical Property:

• PSA: 29.46000
• LogP: 2.09930

Purity/Quality:

95% ^*data from raw suppliers

2-Ethoxy-5-methyl-phenol 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenol, 2-ethoxy-5-methyl-

There total 4 articles about Phenol, 2-ethoxy-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-diethoxy-toluene (2612-56-8) → 2-ethoxy-4-methylphenol (2563-07-7) + 2-ethoxy-5-methylphenol (2563-04-4)

Guidance literature:

With niobium pentachloride; In 1,2-dichloro-ethane; at 20 ℃; for 7h; Title compound not separated from byproducts;

DOI:10.1055/s-2004-817766

Reference yield:

2-ethoxy-5-methylaniline (6331-70-0) → 2-ethoxy-5-methylphenol (2563-04-4)

Guidance literature:

With sulfuric acid; Diazotization_.Einfliessenlassen der Loesung in ein auf 135-140grad erhitztes Gemisch von konz. Schwefelsaeure und Wasser;

Reference yield:

6,6-diacetoxy-4-methyl-cyclohexa-2,4-dienone (7244-03-3) + ethylmagnesium bromide (925-90-6) → 2-ethoxy-5-methylphenol (2563-04-4)

Guidance literature:

With diethyl ether;

DOI:10.1007/BF00899130

upstream raw materials:

6,6-diacetoxy-4-methyl-cyclohexa-2,4-dienone

ethylmagnesium bromide

2-ethoxy-5-methylaniline

3,4-diethoxy-toluene

Downstream raw materials:

(2-ethoxy-5-methyl-phenoxy)-acetic acid

2-Aethoxy-4-tert.-butyl-5-methyl-phenol