3,4-Dimethoxythioanisole

Base Information

Chemical Name:3,4-Dimethoxythioanisole
CAS No.:2570-43-6
Molecular Formula:C9H12O2S
Molecular Weight:184.259
Hs Code.:
European Community (EC) Number:673-600-9
DSSTox Substance ID:DTXSID00948574
Nikkaji Number:J1.809.806G
Wikidata:Q82926400
Mol file:2570-43-6.mol

Synonyms:3,4-Dimethoxythioanisole;2570-43-6;1,2-dimethoxy-4-methylsulfanylbenzene;1,2-dimethoxy-4-(methylsulfanyl)benzene;(3,4-dimethoxyphenyl)(methyl)sulfane;3,4-Dimethoxythioanisol;SCHEMBL3511079;DTXSID00948574;1-(Methylthio)-3,4-dimethoxybenzene;AKOS006278641;E97742

Suppliers and Price of 3,4-Dimethoxythioanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,4-DIMETHOXYTHIOANISOLE 98.00%
50G
$ 2933.70

AHH
3,4-Dimethoxythioanisole 98%
50g
$ 290.00

Total 10 raw suppliers

Chemical Property of 3,4-Dimethoxythioanisole

Chemical Property:

PSA：43.76000
LogP:2.42570
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:184.05580079
Heavy Atom Count:12
Complexity:130

Purity/Quality:

98%min ^*data from raw suppliers

3,4-DIMETHOXYTHIOANISOLE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)SC)OC

Technology Process of 3,4-Dimethoxythioanisole

There total 13 articles about 3,4-Dimethoxythioanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 700-96-9
3,4-dimethoxythiophenol

: 74-88-4
methyl iodide

: 2570-43-6
(3,4-dimethoxyphenyl)(methyl)sulfane

Guidance literature:: With potassium hydroxide; In ethanol; for 0.5h; Inert atmosphere; Reflux;
DOI:10.1021/jacs.0c11420

Reference yield: 80.0%

: 624-92-0
Dimethyldisulphide

: 2859-78-1
4-Bromoveratrole

: 2570-43-6
(3,4-dimethoxyphenyl)(methyl)sulfane

Guidance literature:: 4-Bromoveratrole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

Dimethyldisulphide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jacs.1c00529

Reference yield: 78.0%

: 124-38-9,18923-20-1
carbon dioxide

: 700-96-9
3,4-dimethoxythiophenol

: 2570-43-6
(3,4-dimethoxyphenyl)(methyl)sulfane

Guidance literature:: carbon dioxide; 3,4-dimethoxythiophenol; With sodium tetrahydroborate; 18-crown-6 ether; at 80 ℃; for 0.5h; under 76.0051 Torr; Schlenk technique; Sealed tube;

With iodine; at 140 ℃; for 12h; Schlenk technique; Sealed tube;
DOI:10.1021/acs.joc.9b01180