Phosphinous acid, bis(2-methoxyphenyl)-, methyl ester

Base Information

Chemical Name:Phosphinous acid, bis(2-methoxyphenyl)-, methyl ester
CAS No.:257290-41-8
Molecular Formula:C15H17O3P
Molecular Weight:276.272
Hs Code.:
Mol file:257290-41-8.mol

Synonyms:

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Chemical Property of Phosphinous acid, bis(2-methoxyphenyl)-, methyl ester

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Technology Process of Phosphinous acid, bis(2-methoxyphenyl)-, methyl ester

There total 1 articles about Phosphinous acid, bis(2-methoxyphenyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 103223-33-2
N,N-diethylamino-bis-(o-methoxyphenyl)phosphine

: 257290-41-8
bis (2-methoxyphenyl)methoxyphosphine

Guidance literature:: at 65 ℃; for 4h;
DOI:10.1039/b111629k

Reference yield: 74.0%

: 1167495-01-3
(κ2-O,P-(bis(2-methoxyphenyl)phosphino)benzenesulfonate)(η4-1,5-cyclooctadiene)rhodium(I)

: 201230-82-2
carbon monoxide

: 257290-41-8
bis (2-methoxyphenyl)methoxyphosphine

: 1167495-10-4
(κ2-O,P-(bis(2-methoxyphenyl)phosphino)benzenesulfonate)(bis(2-methohyphenyl)methoxyphosphine)carbonylrhodium(I)

Guidance literature:: In dichloromethane; (N2), Rh complex dissolved in deaerated CH2Cl2 soln., CO bubbled throughthis soln. for 5 min, and then N2 for 5 min, treated with P(OMe)(o-OMeC 6H4)2, stirred for 30 min at room temp.; concd., pptd.(Et2O), washed (Et2O), dried (N2 stream), elem. anal.;
DOI:10.1016/j.molcata.2008.05.013

Reference yield: 28.0%

: 98-11-3
benzenesulfonic acid

: 257290-41-8
bis (2-methoxyphenyl)methoxyphosphine

: 257290-43-0
2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid

Guidance literature:: benzenesulfonic acid; With n-hexyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 20h;

bis (2-methoxyphenyl)methoxyphosphine; In tetrahydrofuran; hexane; at 20 ℃; for 16h; Further stages.;
DOI:10.1039/b111629k