Benzene, (2-methoxy-1-propenyl)-, (E)-

Base Information

Chemical Name:Benzene, (2-methoxy-1-propenyl)-, (E)-
CAS No.:26567-82-8
Molecular Formula:C10H12O
Molecular Weight:148.205
Hs Code.:

Synonyms:(E)-2-methoxy-1-phenylpropene;(E)-2-Methoxy-1-phenyl-propen;((E)-2-Methoxy-propenyl)-benzene;(E)-2-Methoxy-1-phenylpropen;E-2-methoxy-1-phenylpropene;β-Methoxy-trans-β-methylstyrol;

Suppliers and Price of Benzene, (2-methoxy-1-propenyl)-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzene, (2-methoxy-1-propenyl)-, (E)-

Chemical Property:

Boiling Point:207.05 °C (759.8 mmHg)
PSA：9.23000
Density:0.968±0.06 g/cm3(Predicted)
LogP:2.69380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, (2-methoxy-1-propenyl)-, (E)-

There total 8 articles about Benzene, (2-methoxy-1-propenyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: (E)-2-phenyl-1-propenyl(phenyl)iodium (E-2) tetrafluroborate

: 26567-82-8
(2-methoxyprop-1-en-1-yl)benzene

: 4541-69-9
E-α-methoxy-β-methylstyrene

: 58966-08-8
(Z)-(1-methoxyprop-1-en-2-yl)benzene

: 58966-09-9
(E)-(1-methoxyprop-1-en-2-yl)benzene

Guidance literature:: at 60 ℃; Further Variations:; Solvents; Reagents; Temperatures; Reaction partners; Product distribution; Kinetics;
DOI:10.1021/ja010861n

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 67-56-1
methanol

: 26567-83-9
(2-methoxyprop-1-en-1-yl)benzene

: 26567-82-8
(2-methoxyprop-1-en-1-yl)benzene

Guidance literature:: methanol; With potassium hydride; In tetrahydrofuran; at 20 - 50 ℃; for 0.5h; Inert atmosphere;

1-Phenylprop-1-yne; In N,N-dimethyl-formamide; at 55 ℃; for 3h; Overall yield = 51 %;
DOI:10.1016/j.tet.2015.04.038

Reference yield:

: 343986-60-7
2-methoxy-2-methyl-3-phenylpropionic acid

: 26567-82-8
(2-methoxyprop-1-en-1-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide; AIBN / CCl₄ / 0.5 h / Heating

2: diisopropylethylamine / CH₂Cl₂ / 0.02 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/ja0042938