Technology Process of Benzoyl chloride, 2,4-dimethoxy-5-nitro-
There total 5 articles about Benzoyl chloride, 2,4-dimethoxy-5-nitro- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane;
DOI:10.1021/jo050798a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 72 percent / nitric acid; acetic acid / 12 h / 20 °C
2: 64.4 percent / sulfuric acid / Heating
3: 50 percent / potassium carbonate / dimethylformamide / 72 h / 100 °C
4: 96 percent / sodium hydroxide / methanol; H2O / Heating
5: thionyl chloride / 4 h / Heating
With
sodium hydroxide; thionyl chloride; nitric acid; potassium carbonate; acetic acid;
sulfuric acid;
In
methanol; water; N,N-dimethyl-formamide;
1: Substitution / 2: Etherification / 3: Alkylation / 4: Hydrolysis / 5: Substitution;
DOI:10.1021/ja994433h
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 64.4 percent / sulfuric acid / Heating
2: 50 percent / potassium carbonate / dimethylformamide / 72 h / 100 °C
3: 96 percent / sodium hydroxide / methanol; H2O / Heating
4: thionyl chloride / 4 h / Heating
With
sodium hydroxide; thionyl chloride; potassium carbonate;
sulfuric acid;
In
methanol; water; N,N-dimethyl-formamide;
1: Etherification / 2: Alkylation / 3: Hydrolysis / 4: Substitution;
DOI:10.1021/ja994433h
