(S)-(+)-O-Methyl-ethylphenylphosphinothionat

Base Information

• Chemical Name: (S)-(+)-O-Methyl-ethylphenylphosphinothionat
• CAS No.: 38605-14-0
• Molecular Formula: C₉H₁₃OPS
• Molecular Weight: 200.241
• Mol file: 38605-14-0.mol

Synonyms:

Chemical Property of (S)-(+)-O-Methyl-ethylphenylphosphinothionat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-(+)-O-Methyl-ethylphenylphosphinothionat

There total 3 articles about (S)-(+)-O-Methyl-ethylphenylphosphinothionat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methylate (124-41-4) + Dicyclohexyl-amine; compound with (R)-ethyl-phenyl-phosphinothioic acid → (S)-(+)-O-Methyl-ethylphenylphosphinothionat (38605-14-0)

Guidance literature:

Multistep reaction; (i) (EtO)2POCl, benzene, (ii) /BRN= 3592982/, MeOH;

DOI:10.1016/S0040-4020(01)88959-6

Reference yield:

methanol (67-56-1) + ethylphenylphosphinous chloride (15849-83-9,75231-38-8,75231-39-9) → (S)-(+)-O-Methyl-ethylphenylphosphinothionat (38605-14-0)

Guidance literature:

Multistep reaction; (i) (S)-dimethyl-(1-phenyl-ethyl)-amine, (ii) sulfur;

DOI:10.1039/c39750000382

Reference yield:

→ (S)-(+)-O-Methyl-ethylphenylphosphinothionat (38605-14-0)

Guidance literature:

Mischung P^III-Ester 1 u. 2 ((-)-(S)-2 m. NaOMe), Schwefel;

DOI:10.1039/c39760001025

upstream raw materials:

sodium methylate

methanol

ethylphenylphosphinous chloride

Downstream raw materials:

(-)-(S)-S-methyl ethylphenylphosphinothioate