methyl trans-3-p-tolylthio-2-propen-1-oate

Base Information

• Chemical Name: methyl trans-3-p-tolylthio-2-propen-1-oate
• CAS No.: 110793-09-4
• Molecular Formula: C₁₂H₁₄O₂S
• Molecular Weight: 222.308
• Mol file: 110793-09-4.mol

Synonyms:

Chemical Property of methyl trans-3-p-tolylthio-2-propen-1-oate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl trans-3-p-tolylthio-2-propen-1-oate

There total 1 articles about methyl trans-3-p-tolylthio-2-propen-1-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + β-p-tolylthio-α-chloroethyl methyl ether (96856-70-1) + 1-ethoxyacetylene (927-80-0) → methyl trans-3-p-tolylthio-2-propen-1-oate (110793-09-4)

Guidance literature:

With titanium tetrachloride; sodium hydrogencarbonate; potassium carbonate; Yield given. Multistep reaction; 1.) CH2Cl2, -70 deg C, 1 h, 2.) -70 -> -30 deg C, 20 min;

DOI:10.1007/BF00953857

upstream raw materials:

methanol

β-p-tolylthio-α-chloroethyl methyl ether

1-ethoxyacetylene