Introduce the CO source into the reaction vessel under an inert atmosphere. This could be done by either using a CO gas cylinder or a CO-releasing reagent. Maintain the reaction mixture at an appropriate temperature and pressure for carbonylation to occur. Typically, this is done under elevated pressure (high-pressure reactor) and at an elevated temperature, usually in the range of 100-150°C.
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Propanoic acid, phenyl ester, labeled with carbon-14 (9CI)
CO
[11C-carbonyl]triclocarban
Palladium, diiodobis(2-isocyano-1,3-dimethylbenzene)-
3-[1,3]-dioxolan-2-ylthiopropionic acid S-phenyl ester
CO
