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(+)-D-glucosamine hydrochloride
uranyl acetate
caesium carbonate
salicylaldehyde
Conditions | Yield |
---|---|
Stage #1: uranyl acetate; salicylaldehyde In methanol at 20℃; for 2h; Stage #2: (+)-D-glucosamine hydrochloride In methanol; water at 20℃; for 1.5h; Stage #3: caesium carbonate In methanol; water at 20℃; for 18.5h; | 91% |
water
uranyl acetate
1,2-diamino-benzene
2-hydroxynaphthalene-1-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 1,2-diamino-benzene; 2-hydroxynaphthalene-1-carbaldehyde In methanol Reflux; Stage #2: uranyl acetate at 65℃; for 5h; Reflux; Stage #3: water | 85% |
methanol
uranyl acetate
4-Nitrophenylene-1,2-diamine
2-hydroxynaphthalene-1-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: methanol; 4-Nitrophenylene-1,2-diamine; 2-hydroxynaphthalene-1-carbaldehyde Reflux; Stage #2: uranyl acetate at 65℃; for 5h; Reflux; | 85% |
Conditions | Yield |
---|---|
Stage #1: methanol; salicylaldehyde; 4-Nitrophenylene-1,2-diamine Reflux; Stage #2: uranyl acetate at 65℃; for 5h; Reflux; | 75% |
Conditions | Yield |
---|---|
Stage #1: methanol; 5-Nitrosalicylaldehyde; 1,2-diamino-benzene Reflux; Stage #2: uranyl acetate at 65℃; for 5h; Reflux; | 70% |
methanol
uranyl acetate
5-Nitrosalicylaldehyde
4-Nitrophenylene-1,2-diamine
Conditions | Yield |
---|---|
Stage #1: methanol; 5-Nitrosalicylaldehyde; 4-Nitrophenylene-1,2-diamine Reflux; Stage #2: uranyl acetate at 65℃; for 5h; Reflux; | 60% |
1-(D-glucopyranosyl-2'-deoxy-2'-iminomethyl)-2-hydroxybenzene
uranyl acetate
caesium carbonate
Conditions | Yield |
---|---|
Stage #1: 1-(D-glucopyranosyl-2'-deoxy-2'-iminomethyl)-2-hydroxybenzene; uranyl acetate In methanol at 20℃; for 2h; Inert atmosphere; Stage #2: caesium carbonate In methanol Inert atmosphere; | 57% |
Conditions | Yield |
---|---|
With ammonia |
Chemistry informtion about Uranium Oxyacetate (CAS NO.541-09-3) is:
IUPAC Name: Acetic Acid; Dioxouranium
Synonyms: Uranylacetate,A.C.S.Grade ; Uranium, Bis(Acetato-.Kappa.O)Dioxo-, (T-4)- ; Uranium,Bis(Aceto)Dioxo- ; Uranylethanoate ; Uranyl Acetate, Anhydrous ; Uranium, Bis(Acetato-O)Dioxo- ; Uranyl Acetate: (Uranium Oxyacetate) ; Bis(Acetato)Dioxo-Uraniu
Product Categories: Organic-metal salt
MF: C4H8O6U
MW: 388.12
EINECS: 208-767-5
Density: 2.89 g / cm3
Flash Point: 40 °C
Boiling Point: 117.1 °C at 760 mmHg Vapour Pressure: 13.9 mmHg at 25°C
Enthalpy of Vaporization: 23.7 kJ/mol
Following is the molecular structure of Uranium Oxyacetate (CAS NO.541-09-3) is:
Uranium Oxyacetate (CAS NO.541-09-3) is used as a negative stain in electron microscopy. In fact, most procedures in electron microscopy for biology require the use of uranyl acetate. In the negative staining method 1 or 2% aqueous solution is normally being used. One of the most advantage of the type of staining is its simplicity, one can examine the sample within a few minutes after staining. Some biological samples may be adversely affected by uranyl acetate staining and, in these cases, a low voltage electron microscopy technique may be more suitable due to the improved resolution of low atomic number materials. 1% and 2% Uranyl Acetate solutions are used as an indicator, and a titrant in stronger concentrations in analytical chemistry, as it forms an insoluble salt with sodium (the vast majority of sodium salts are water-soluble). Uranyl Acetate solutions show evidence of being sensitive to light, especially UV and will precipitate if exposed. Uranyl Acetate is also used in a standard test—American Association of State Highway and Transportation Officials (AASHTO) Designation T 299—for alkali-silica reactivity in aggregates (crushed stone or gravel) being considered for use in cement concrete.
Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
---|---|---|---|---|---|
mouse | LD50 | intraperitoneal | 24mg/kg (24mg/kg) | Journal of Toxicology and Environmental Health. Vol. 11, Pg. 237, 1983. |
Reported in EPA TSCA Inventory.
Poison by intraperitoneal route. A radioactive material. See also URANIUM.
RIDADR: 2912
HazardClass: 7
PackingGroup: III
OSHA PEL: TWA 0.05 mg(U)/m3
ACGIH TLV: TWA 0.2 mg(U)/m3
Uranium Oxyacetate (CAS NO.541-09-3) is a yellow crystals with a slight odor of vinegar. It can soluble in water and reacting to give a milky solution. The reaction is not hazardous. It reacts weakly as an acid. Usually does not react as either oxidizing agents or reducing agents but such behavior is not impossible. May catalyze organic reactions. Inhalation of dust may irritate nose and throat. Contact with eyes causes irritation.