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Basic Information
CAS No.: 101372-99-0
Name: 4,6,10-Hexadecatrien-1-ol, acetate, (E,E,Z)-
Molecular Structure:
Molecular Structure of 101372-99-0 (4,6,10-Hexadecatrien-1-ol, acetate, (E,E,Z)-)
Formula: C18H30O2
Molecular Weight: 278.435
Synonyms: (E,E,Z)-4,6,10-hexadecatrienyl acetate;(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate;4,6,10-Hexadecatrien-1-ol,acetate,(E,E,Z);
PSA: 57.53000
LogP: 4.87890
Related products
Synthetic route
101373-01-7

(4E,6E,10Z)-hexadeca-4,6,10-trien-1-ol

108-24-7

acetic anhydride

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
With pyridine at 20℃; Concentration; Inert atmosphere;97%
108-24-7

acetic anhydride

101373-00-6, 101373-01-7, 142143-85-9

(E,Z)-4,6,10-hexadecatrienyl alcohol

A

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

B

139650-81-0

(4E,6Z,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
With pyridine Ambient temperature; Yield given. Yields of byproduct given;
...Expand
30390-50-2, 65405-70-1, 21662-09-9

(Z)-4-decenal

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, RT, 30 min
2: PPTs / methanol / 24 h / Ambient temperature
3: pyridine / Ambient temperature
View Scheme
142143-84-8, 142143-87-1

1-<(tetrahydropyranyl)oxy>-(4E,10Z)-hexadecatriene

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: PPTs / methanol / 24 h / Ambient temperature
2: pyridine / Ambient temperature
View Scheme
144054-75-1

(Z)-4-decenyltriphenylphosphonium bromide

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) t-BuOK / 1.) THF, -30 deg C, 30 min, 2.) THF, 2 h
2: PPTs / methanol / 24 h / Ambient temperature
3: pyridine / Ambient temperature
View Scheme
144054-76-2

6-<(tetrahydropyranyl)oxy>-2E-hexanetriphenylphosphonium bromide

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, RT, 30 min
2: PPTs / methanol / 24 h / Ambient temperature
3: pyridine / Ambient temperature
View Scheme

(6E,10Z)-1-tetrahydropyran-2-yloxy-hexadecadiene-4-yne

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 20 °C
2: lithium; ammonium hydroxide
3: pyridine / 20 °C / Inert atmosphere
View Scheme

(6E,10Z)-hexadecadiene-4-yn-1-ol

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium; ammonium hydroxide
2: pyridine / 20 °C / Inert atmosphere
View Scheme
5390-04-5

pent-1-yn-5-ol

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 0 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; diisopropylamine / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere
3.1: iron(III)-acetylacetonate; 1-methyl-pyrrolidin-2-one / tetrahydrofuran / -20 - -15 °C / Inert atmosphere
3.2: 8 h / -15 - 20 °C / Inert atmosphere
4.1: toluene-4-sulfonic acid / methanol / 20 °C
5.1: lithium; ammonium hydroxide
6.1: pyridine / 20 °C / Inert atmosphere
View Scheme
62992-46-5

1-(tetrahydropyranyloxy)-4-pentyn

101372-99-0

(4E,6E,10Z)-4,6,10-hexadecatrienyl acetate

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; diisopropylamine / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere
2.1: iron(III)-acetylacetonate; 1-methyl-pyrrolidin-2-one / tetrahydrofuran / -20 - -15 °C / Inert atmosphere
2.2: 8 h / -15 - 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / methanol / 20 °C
4.1: lithium; ammonium hydroxide
5.1: pyridine / 20 °C / Inert atmosphere
View Scheme
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