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Basic Information
| CAS No.: | 10304-09-3 |
|---|---|
| Name: | methoxy(oxo)acetic acid |
| Article Data: | 4 |
| Molecular Structure: | |
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| Formula: | C3H4 O4 . K |
| Molecular Weight: | 142.153 |
| Synonyms: | Ethanedioicacid, monomethyl ester, potassium salt (9CI); Oxalic acid, methyl ester,potassium salt (7CI,8CI); Monomethyl oxalate potassium salt; Potassium methyloxalate |
| Density: | 1.366g/cm3 |
| Boiling Point: | 192.9°C at 760 mmHg |
| Flash Point: | 88.9°C |
| PSA: | 63.60000 |
| LogP: | -0.75600 |
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Synthetic route
- 553-90-2
Dimethyl oxalate
- 10304-09-3
potassium oxalate monomethyl ester
Conditions
| Conditions | Yield |
|---|---|
| With potassium acetate In methanol; water at 80℃; for 3h; | 100% |
| With potassium acetate In methanol; water at 80℃; for 3h; | 91% |
| With potassium acetate In methanol; water at 60℃; for 1h; | 80% |
| With potassium acetate In methanol; water at 90℃; for 2h; Reflux; |
- 10304-09-3
potassium oxalate monomethyl ester
- 1482-97-9, 6018-55-9, 6018-56-0, 19777-68-5, 19777-69-6, 28843-13-2, 54897-59-5, 69531-11-9, 125767-61-5
(2R)-2,3-diaminopropanoic acid monohydrochloride
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: (2R)-2,3-diaminopropanoic acid monohydrochloride With lithium hydroxide monohydrate In methanol; water for 1h; Cooling with ice; Stage #2: potassium oxalate monomethyl ester In methanol; water at 20℃; for 18h; Concentration; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| With 1,3-bis-(diphenylphosphino)propane; palladium dichloride In 1-methyl-pyrrolidin-2-one at 150℃; for 24h; Inert atmosphere; Schlenk technique; | 75% |
- 894-08-6
triphenylplumbyl hydroxide
- 10304-09-3
potassium oxalate monomethyl ester
- 107399-19-9
(C6H5)3PbO2CCO2CH3
Conditions
| Conditions | Yield |
|---|---|
| With methanol In methanol HO2CCO2CH3 prepared in situ from potassium salt in methanol, pptd. at room temp. by equimolar amount of R3MOH; suspn. in CH3OH warmed, solvent vol. reduced; elem. anal.; | 74% |
- 10304-09-3
potassium oxalate monomethyl ester
- 17546-98-4
Trimethylbleimonohydroxyd
- 107399-17-7
(CH3)3PbO2CCO2CH3
Conditions
| Conditions | Yield |
|---|---|
| With methanol In methanol HO2CCO2CH3 prepared in situ from potassium salt in methanol, pptd. at room temp. by equimolar amount of R3MOH; suspn. in CH3OH warmed, solvent vol. reduced; elem. anal.; | 70% |
- 76-87-9
triphenyltin(IV) hydroxide
- 10304-09-3
potassium oxalate monomethyl ester
- 107399-18-8
(C6H5)3SnO2CCO2CH3
Conditions
| Conditions | Yield |
|---|---|
| With methanol In methanol HO2CCO2CH3 prepared in situ from potassium salt in methanol, pptd. at room temp. by equimolar amount of R3MOH; suspn. in CH3OH warmed, solvent vol. reduced; elem. anal.; | 65% |
- 10304-09-3
potassium oxalate monomethyl ester
- 56-24-6
trimethyltin(IV) hydroxide
- 107399-16-6
(CH3)3SnO2CCO2CH3
Conditions
| Conditions | Yield |
|---|---|
| With methanol In methanol HO2CCO2CH3 prepared in situ from potassium salt and methanol, pptd. at room temp. by equimolar amount R3MOH; suspn. in CH3OH warmed, solvent vol. reduced; elem. anal.; | 56% |
- 106-38-7
para-bromotoluene
- 10304-09-3
potassium oxalate monomethyl ester
- 99-75-2
4-methyl-benzoic acid methyl ester
Conditions
| Conditions | Yield |
|---|---|
| With palladium(II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane In 1-methyl-pyrrolidin-2-one at 150℃; for 24h; Inert atmosphere; | 52% |
- 615-96-3
Ethyl 2-bromohexanoate
- 10304-09-3
potassium oxalate monomethyl ester
Conditions
| Conditions | Yield |
|---|---|
| In dimethyl sulfoxide at 20℃; for 48h; Inert atmosphere; | 49% |
- 5781-53-3
monomethyl oxalyl chloride
- 10304-09-3
potassium oxalate monomethyl ester
- 5781-55-5
methoxalic anhydride
Conditions
| Conditions | Yield |
|---|---|
| (i) aq. KOAc, MeOH, (ii) /BRN= 1071541/, benzene,; Multistep reaction; |
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methoxy(oxo)acetic acid
