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CAS No.: | 10351-88-9 |
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Name: | PHYLLANTHIN |
Article Data: | 3 |
Molecular Structure: | |
Formula: | C24H34 O6 |
Molecular Weight: | 418.53 |
Synonyms: | Benzene,1,1'-[2,3-bis(methoxymethyl)-1,4-butanediyl]bis[3,4-dimethoxy-, [S-(R*,R*)]-;Butane, 1,4-dimethoxy-2,3-diveratryl-, (2S,3S)-(+)- (8CI); Phyllanthin (7CI);NSC 619043 |
Density: | 1.069g/cm3 |
Melting Point: | 96℃ |
Boiling Point: | 530.6°Cat760mmHg |
Flash Point: | 207.3°C |
PSA: | 55.38000 |
LogP: | 4.03140 |
Dg-threo-2,3-bis-(3,4-dimethoxy-benzyl)-butanediol-(1,4)
methyl iodide
(+)-phyllanthin
Conditions | Yield |
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With silver(l) oxide In N,N-dimethyl-formamide |
Conditions | Yield |
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(i) Li, EtOH, liq. NH3, (ii) NaH, benzene, (iii) /BRN= 969135/; Multistep reaction; |
Conditions | Yield |
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With sodium hydride |
Dg-threo-2.3-bis-(3.4-dimethoxy-benzyl)-succinic acid
(+)-phyllanthin
Conditions | Yield |
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Multi-step reaction with 3 steps 2: LiAlH4 / tetrahydrofuran 3: Ag2O / dimethylformamide View Scheme |
D,L-2,3-bis(3,4-dimethoxybenzyl)succinic acid
(+)-phyllanthin
Conditions | Yield |
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Multi-step reaction with 4 steps 3: LiAlH4 / tetrahydrofuran 4: Ag2O / dimethylformamide View Scheme |
(+)-phyllanthin
Conditions | Yield |
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Multi-step reaction with 2 steps 1: LiAlH4 / tetrahydrofuran 2: Ag2O / dimethylformamide View Scheme |
(+)-phyllanthin
4-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-3-methoxymethyl-naphthalene-2-carbaldehyde
Conditions | Yield |
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With acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone at 50℃; for 0.666667h; sonication; | 92% |
(+)-phyllanthin
3,4,3',4'-tetramethoxy-9,9'-epoxylignan
Conditions | Yield |
---|---|
With trifluoroacetic anhydride; trichlorophosphate In benzene for 6h; Heating; | 45% |
(+)-phyllanthin
(S:S)-1,4-dimethoxy-2,3-bis-(6-bromo-3,4-dimethoxy-benzyl)-butane
Conditions | Yield |
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With chloroform; bromine |
(+)-phyllanthin
Conditions | Yield |
---|---|
With nitric acid In acetic acid |