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1062580-52-2

Basic Information
CAS No.: 1062580-52-2
Name: CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)
Article Data: 6
Molecular Structure:
Molecular Structure of 1062580-52-2 (CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE))
Formula: C14H24Cl2N2
Molecular Weight: 291.264
Synonyms: (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidi;
Melting Point: 249~251℃
PSA: 15.27000
LogP: 4.04920
Synthetic route
477600-70-7

N-(3R,4R)-(1-benzyl-4-methylpiperidin-3-yl)-methylamine

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 0 - 5℃; pH=3 - 4;94%
With hydrogenchloride In n-heptane; isopropyl alcohol at 20℃; for 0.666667h; Reflux;60%
32018-96-5

1-benzyl-4-methyl-piperidin-3-one

74-89-5

methylamine

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
Stage #1: 1-benzyl-4-methyl-piperidin-3-one; methylamine With titanium tetrachloride; triethylamine In tetrahydrofuran at 20℃; for 4h;
Stage #2: With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran at 25℃;
Stage #3: With hydrogenchloride In ethanol
85%
32018-96-5

1-benzyl-4-methyl-piperidin-3-one

6998-30-7

methylamine acetate

A

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

B

(3R,4R)-1-benzyl-N,4-dimethylpiperidine-3-amine dihydrochloride

Conditions
ConditionsYield
Stage #1: 1-benzyl-4-methyl-piperidin-3-one; methylamine acetate With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (S)-3,5-di-tert-butyl-4-methoxyphenyl-(6,6’-dimethoxybiphenyl-2,2’-diyl)-bis(diphenylphosphine); hydrogen In dichloromethane; isopropyl alcohol at 70℃; under 37503.8 Torr; for 18h;
Stage #2: With hydrogenchloride In dichloromethane; water; isopropyl alcohol Overall yield = 86%; Overall yield = 498 mg; enantioselective reaction;
A n/a
B 74%
384338-23-2

(1-benzyl-4-methyl-piperidin-3-yl)-methyl-amine

A

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

B

(3R,4R)-1-benzyl-N,4-dimethylpiperidine-3-amine dihydrochloride

Conditions
ConditionsYield
With hydrogenchloride In diethyl ether; acetone for 1h; Inert atmosphere; Overall yield = 498 mg;
32018-96-5

1-benzyl-4-methyl-piperidin-3-one

A

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

B

(3R,4R)-1-benzyl-N,4-dimethylpiperidine-3-amine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ethanol / 5 h / 20 °C / Inert atmosphere
2: hydrogen; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-diMe-PipPhos / isopropyl alcohol / 18 h / 20 °C / 37503.8 Torr / Glovebox; Inert atmosphere
3: hydrogenchloride / acetone; diethyl ether / 1 h / Inert atmosphere
View Scheme

C14H20N2

A

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

B

(3R,4R)-1-benzyl-N,4-dimethylpiperidine-3-amine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-diMe-PipPhos / isopropyl alcohol / 18 h / 20 °C / 37503.8 Torr / Glovebox; Inert atmosphere
2: hydrogenchloride / acetone; diethyl ether / 1 h / Inert atmosphere
View Scheme

methyl ((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)carbamate

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 2.83 h / 0 °C / Reflux
2: hydrogenchloride / isopropyl alcohol; n-heptane / 0.67 h / 20 °C / Reflux
View Scheme
923036-28-6

(1-benzyl-4-methyl-1,2,5,6-tetrahydropyridin-3-yl)carbamic acid methyl ester

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrogen; bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; (R)-1-[(Sp)-2-(di-tert-butylphosphino)ferrocenyl]ethylbis(2-methylphenyl)phosphine / 2,2,2-trifluoroethanol / 6 h / 30 - 50 °C / 2625.26 Torr
2: lithium aluminium tetrahydride / tetrahydrofuran / 2.83 h / 0 °C / Reflux
3: hydrogenchloride / isopropyl alcohol; n-heptane / 0.67 h / 20 °C / Reflux
View Scheme
3430-27-1

3-amino-4-methylpyridine

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: dichloromethane; toluene / 10 h / 20 - 25 °C / Large scale
1.2: 70 - 80 °C / Large scale
1.3: 14 h / 10 °C / Large scale
2.1: hydrogenchloride / water; n-heptane / 70 - 75 °C / Large scale
2.2: 0 - 5 °C / Large scale
3.1: Di-p-toluoyl-L-tartaric acid / methanol / 1 h / 50 - 55 °C / Large scale
3.2: 2 h / pH 3 / Large scale
View Scheme

N-(1-benzyl-4-methyl-1,2,5,6-tetrahydropyridine-3-yl)acetylamine

1062580-52-2

N-((3R,4R)-1-benzyl-4-methylpiperidin-3-yl)-N-methylamine dihydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: hydrogenchloride / water; n-heptane / 70 - 75 °C / Large scale
1.2: 0 - 5 °C / Large scale
2.1: Di-p-toluoyl-L-tartaric acid / methanol / 1 h / 50 - 55 °C / Large scale
2.2: 2 h / pH 3 / Large scale
View Scheme
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  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

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    CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

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  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINEDITYDROCHLORIDE

  • Casno:

    1062580-52-2

    (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINEDITYDROCHLORIDE

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • cis-1-Benzyl-3-(methylamino)-4-methylpiperidine Dihydrochloride

  • Casno:

    1062580-52-2

    cis-1-Benzyl-3-(methylamino)-4-methylpiperidine Dihydrochloride

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

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    1062580-52-2

    CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

    Min.Order: 1 Gram

    FOB Price:  USD $ 1.0-1.0

    Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

    Shanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We sp

  •  Shanghai Massive Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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  • (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORIDE

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    1062580-52-2

    (3R,4R)-1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORIDE

    Min.Order: 10 Gram

    FOB Price:  USD $ 100.0-100.0

    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

  •  Zibo Hangyu Biotechnology Development Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

  • Casno:

    1062580-52-2

    CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

    Zibo Dorne chemical technology co., LTD. is a biotechnology enterprise engaged in the R&D, production and sales of drugs, steroids, peptides, raw materials, vitamins, food additive

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-18560316533

    Address:No. 416, 4th floor, zhongguancun science and technology city, no. 1, west 6th road, zhangdian district

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  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidi

  • Casno:

    1062580-52-2

    (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidi

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Product Name: CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE) Synonyms: CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROC…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton

    Kono Chem Co.,Ltd is a leading producer of standardized herbal extracts, natural active ingredients and APIs for pharmaceutical, health food and cosmetic industries. Annually, mo

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-29-86107037-8015

    Address:No.11 Daqing Road,Lianhu District,Xi’an 710082,China

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  • CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

  • Casno:

    1062580-52-2

    CIS-N-BENZYL-3-METHYLAMINO-4-METHYL-PIPERIDINE BIS-(HYDROCHLORIDE)

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 18.0-20.0

    factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

  •  EAST CHEMSOURCES LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15053231572

    Address:No.1581-12,Jinshui Road, Licang, Qingdao,China

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  • Lower Price (3R,4R)-N,4-Dimethyl-1-(Phenylmethyl)-3-Piperidinamine Hydrochloride

  • Casno:

    1062580-52-2

    Lower Price (3R,4R)-N,4-Dimethyl-1-(Phenylmethyl)-3-Piperidinamine Hydrochloride

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Product name: (3R,4R)-N,4-Dimethyl-1-(Phenylmethyl)-3-Piperidinamine Hydrochloride CAS No.: 1062580-52-2 Molecule Formula:C14H22N2·2(HCl) Molecule Weight:291.26 Purity: 99.0% Package: 25kg/drum Description:White powder Manufact

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

  •  Siwei Development Group Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-82881840

    Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

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  • 1062580-52-2  CAS NO.1062580-52-2

  • Casno:

    1062580-52-2

    1062580-52-2 CAS NO.1062580-52-2

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 7.0-8.0

    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

    KAISA GROUP INC.is the enterprise which is specialize in manfacturing and exporting avariety of Chemical in China. We have the strong economic base and comprehensive technology.We

  •  KAISA GROUP INC

    United States  |  Contact Details

    Business Type:Trading Company

    Tel:15131197030

    Address:1312 17th Street Suite 1402 Denver CO 80202

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  • (3R,4R)-n,4-dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride

  • Casno:

    1062580-52-2

    (3R,4R)-n,4-dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

    Located in Hangzhou National Hi-Tech Industrial Development Zone, Hangzhou zhongqi chem co.,Ltd is an ISO 9001:2015 & SGS certified molden chemical company,who is mainly focus on t

  •  Hangzhou Zhongqi chem Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:0086-571-86976032

    Address:Kangkang Gu 1010, Chun xiao road 61,Binjiang District 310052,Hangzhou city , China

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  • SAGECHEM/ cis-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride  /Manufacturer in China

  • Casno:

    1062580-52-2

    SAGECHEM/ cis-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride /Manufacturer in China

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

    SAGECHEM is a chemical R&D, manufacturing and distribution company since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and

  •  SAGECHEM LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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  • (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride

  • Casno:

    1062580-52-2

    (3R,4R)-N,4-Dimethyl-1-(phenylmethyl)-3-piperidinamine hydrochloride

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:Active Pharmaceutical I

    Suzhou Health Chemicals Co., Ltd. is A Fine Chemicals Company, specializing in research, development, manufacture and distribute raw materials for pharmaceutical, healthcare, bioch

  •  Suzhou Health Chemicals Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-512-58277800

    Address:No. 338, Jingang Avenue,

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  • (3R,4R)-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride

  • Casno:

    1062580-52-2

    (3R,4R)-1-Benzyl-N,4-dimethylpiperidin-3-amine dihydrochloride

    Min.Order: 25 Gram

    FOB Price:  USD $ 0.0-0.0

    Shanghai Sikuo Chemical Technology Co., Ltd. was established in 2012 and is a chemical supplier that integrates research and development, production, and sales. Dedicated to providing basic chemical, fine chemical, pesticide, and pharmaceutical inter

    Founded in 2012, Shanghai Scochem Technology Co., Ltd.?is a high-tech enterprise integrating R&D, production and sales. It’s located in Zhangjiang Hi-tech Park of Shanghai. We are

  •  Shanghai Scochem Technology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:021-33758897

    Address:3rd Building, Hua Yi Road 76 Zhangjiang Pudong New Area Shanghai, China

       Inquiry Now

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R20:Harmful by inhalation.