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Basic Information
CAS No.: 109428-30-0
Name: 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol
Molecular Structure:
Molecular Structure of 109428-30-0 (1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol)
Formula: C13H14 O4
Molecular Weight: 234.252
Synonyms: Allitol,1,5:2,3-dianhydro-4,6-O-benzylidene- (6CI)
PSA: 40.22000
LogP: 1.26680
Related products
Synthetic route

(4aR,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxine

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

Conditions
ConditionsYield
Stage #1: (4aR,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxine With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; for 1h;
Stage #2: With dimethylsulfide for 0.166667h;		38%

4-Methyl-benzoic acid (4aR,7S,8R,8aR)-2-phenyl-8-(toluene-4-sulfonyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

Conditions
ConditionsYield
With sodium methylate In toluene at 50℃; Yield given;
109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

921772-44-3

1,5-anhydro-2-azido-4,6-O-benzylidene-2-deoxy-D-altritol

Conditions
ConditionsYield
With sodium azide; ammonium chloride In 2-methoxy-ethanol; water at 100℃; for 18h;95%
With sodium azide; ammonium chloride In 2-methoxy-ethanol; water at 100℃; for 18h; Inert atmosphere;95%
66-22-8

uracil

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

181711-37-5

1-((4aR,7R,8S,8aS)-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 120℃;69%
Stage #1: uracil With sodium hydride In DMF (N,N-dimethyl-formamide) for 1h; Heating / reflux;
Stage #2: 1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol In DMF (N,N-dimethyl-formamide) for 24h; Heating / reflux;		29%
2622-05-1

allylmagnesium bromide

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

(4aR,7R,8S,8aS)-7-allyl-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-8-ol

Conditions
ConditionsYield
Stage #1: allylmagnesium bromide With copper(l) iodide In tetrahydrofuran at -30℃; for 0.25h; Inert atmosphere;
Stage #2: 1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol In tetrahydrofuran at -30℃; for 1.5h; Inert atmosphere; regioselective reaction;		69%
With copper(l) iodide In tetrahydrofuran at -30℃; for 1.5h; Inert atmosphere;69%
66224-66-6, 66224-67-7, 66224-68-8, 66224-69-9, 134434-48-3, 134434-49-4, 134454-76-5, 134461-75-9

adenine

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

168696-01-3

(4aR,7R,8S,8aS)-7-(6-Amino-purin-9-yl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 100℃;54%
65-71-4

thymin

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

1-((4aR,7R,8S,8aS)-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-5-methyl-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
Stage #1: thymin With sodium hydride In DMF (N,N-dimethyl-formamide) for 2h; Heating / reflux;
Stage #2: 1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol In DMF (N,N-dimethyl-formamide) for 24h; Heating / reflux;		47%
1517-05-1

2-azidoethanol

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

(4aR,7R,8S,8aS)-7-(2-azidoethoxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-8-ol

Conditions
ConditionsYield
Stage #1: 2-azidoethanol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Inert atmosphere;
Stage #2: 1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol In N,N-dimethyl-formamide; mineral oil at 0 - 80℃; Inert atmosphere;		45%
696-07-1

5-iodouracil

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

1-((4aR,7R,8S,8aS)-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-5-iodo-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
Stage #1: 5-iodouracil With sodium hydride In DMF (N,N-dimethyl-formamide) for 2h; Heating / reflux;
Stage #2: 1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol In DMF (N,N-dimethyl-formamide) for 24h; Heating / reflux;		20%
87-42-3

6-chloropurine

109428-30-0

1,5:2,3-anhydro-4,6-O-benzylidene-D-allitol

(4aR,7R,8S,8aS)-7-(6-Chloro-purin-9-yl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 48h;16%
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  • (7ar,7bs)-6-phenyl-1a,2,3a,4,7a,7b-hexahydrooxireno[1,2]pyrano[3,5-d][1,3]dioxine

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    109428-30-0

    (7ar,7bs)-6-phenyl-1a,2,3a,4,7a,7b-hexahydrooxireno[1,2]pyrano[3,5-d][1,3]dioxine

    Min.Order: 2 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Henan Coreychem co., LTD focus on high complex new type intermediates and fine chemical custom synthesis,scale-up production and rare chemicals trade.Product category including Intermediates&API,Catalyst and Electronic Chemicals.Covering 811 square m

    Career Henan Chemical Co, based on the original Zhengzhou Cote Chemical Research Institute, be brave in absorbing highly educated talents & overseas returnees; actively responded t

  • Career Henan Chemical Co

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-86658258

    Address:Building 10 of Innovation Park, East District of the National University Science Park

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  • 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

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    109428-30-0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

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    High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality produc

    Henan Kanbei Chemical Co., Ltd. is a modern high-tech chemical enterprise integrating R&D, production and sales. The company has strong technical strength, advanced equipment, stri

  • Henan Kanbei Chemical Co.,LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

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  • D-Allitol,1,5:2,3-dianhydro-4,6-O-(phenylmethylene)-

  • Casno:

    109428-30-0

    D-Allitol,1,5:2,3-dianhydro-4,6-O-(phenylmethylene)-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

    United Scientific Company (USC) Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. USC has both the expertise and flexibility

  • Shanghai united Scientific Co.,Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-53535353

    Address:28F No.900 huaihai Road Shanghai China

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  • (1aS,3aR,7aR,7bS)-6-Phenylhexahydrooxireno[2',3':4,5]pyrano[3,2-d][1,3]dioxine

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    109428-30-0

    (1aS,3aR,7aR,7bS)-6-Phenylhexahydrooxireno[2',3':4,5]pyrano[3,2-d][1,3]dioxine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Cool Pharm Ltd, found in 8573,is a high-tech enterprise which provides customer synthesis service for domestic and international pharmaceutical companies according to international standards. Our business includes research , development, process opti

    Jinan YSPharma Biotechnology Co., Ltd is a large group specializing in contract manufacturing to the pharmaceutical, agrochemical and Fine chemicals with top quality products and s

  • coolpharm Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-531-8233381 86-18678657237

    Address:Room 302,Building 1,Union Fortune Square, No. 2117,Tianchen Road,High-tech Zone,Jinan,Shandong,China

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  • 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

  • Casno:

    109428-30-0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

    Chemical Technology Co.,LTD is a professional enterprise which engaged in pharmaceutical intermediates, material intermediates production research and development.Company foc

  • Chemical Technology Co.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Other

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  • 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

  • Casno:

    109428-30-0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

  • Taizhou volsen chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

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  • D-Allitol,1,5:2,3-dianhydro-4,6-O-(phenylmethylene)-

  • Casno:

    109428-30-0

    D-Allitol,1,5:2,3-dianhydro-4,6-O-(phenylmethylene)-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    D-Allitol,1,5:2,3-dianhydro-4,6-O-(phenylmethylene)- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port

    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

  • Nanjing Raymon Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-025-52181296

    Address:Block B, No. 918, Shuanglong Avenue

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  • 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

  • Casno:

    109428-30-0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Do best quality products, erect the morality model Application:please email us, thanks

    Wuxi Morality Chemical Co., Ltd is specialized in the development and manufacture of industrial additives, bulk chemical intermediates, pharmaceutical raw materials and pesticide

  • Wuxi Morality Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-510-83597286 17768505220

    Address:B/7F, 321th WuYun Rd, Wanda Plaza, Wuxi City, 214174, China

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  • 1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

  • Casno:

    109428-30-0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitol

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1,5:2,3-Dianhydro-4,6-O-benzylidene-D-allitolAppearance:white powder Storage:Shading, sealed, dry place. Package:aluminous bag Application:API Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airpor

    Hunan Runhui Chem Co., Ltd. is a comprehensive Fine chemicals and Pharmaceuticals Intermediates supplier in China , Established in Changsha City of Hunan province registered capit

  • Hunan Longxianng Runhui Trading Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-731-85570686

    Address:29 Floor,Changsheng Upper Strata,Furong District,China

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  • 109428-30-0

  • Casno:

    109428-30-0

    109428-30-0

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Supply top quality products with a reasonable price Application:api

    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

  • Hebei Ruishun Trade Co.,Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-311-68037669

    Address:WanDa commerce building ,yuhua district

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