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1223403-58-4

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Basic Information
CAS No.: 1223403-58-4
Name: LOXO-101
Article Data: 4
Molecular Structure:
Molecular Structure of 1223403-58-4 (LOXO-101)
Formula: C21H22F2N6O2
Molecular Weight: 428.441
Synonyms: LOXO-101;(R)-N-(5-((S)-2-(2,5-difluorophenyl)pyrrolidin-1-yl)pyrazolo[1,5-a]pyrimidin-3-yl)-3-hydroxypyrrolidine-1-carboxamide;(3S)-N-[5-[(2R)-2-(2,5-Difluorophenyl)-1-pyrrolidinyl]pyrazolo[1,5-a]pyrimidin-3-yl]-3-hydroxy-1-pyrrolidinecarboxamide;ARRY 470;Larotrectinib
Density: 1.55±0.1 g/cm3(Predicted)
Appearance: White to yellow solid
PSA: 86.00000
LogP: 3.02340
Related products
Synthetic route
1223404-88-3

(R)-5-(2-(2,5-difluorophenyl)pyrrolidin-1-yl)pyrazolo[1,5-a]pyrimidine-3-amine

100243-39-8

3-hydroxypyrrolidine

530-62-1

1,1'-carbonyldiimidazole

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Stage #1: 5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidin-3-amine; 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h;
Stage #2: 3-hydroxypyrrolidine In dichloromethane for 0.0833333h;		91%
...Expand

phenyl (5-((R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl)-3,3a-dihydropyrazolo[1,5-a]pyrimidin-3-yl)carbamate

100243-39-8

3-hydroxypyrrolidine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 75℃; for 6h;91%
1218935-59-1

(R)-(+)-2-(2,5-difluorophenyl)pyrrolidine

(S)-N-(5-chloropyrazolo[1,5-a]pyrimidin-3-yl)-3-hydroxypyrrolidine-1-carboxamide

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In ethanol at 30℃;85%

3-nitro-5-chloropyrazole[1,5-a]pyrimidine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: ammonium chloride; iron / ethanol; water / Inert atmosphere; Reflux
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 10 °C
3: ethanol / 25 °C
4: N-ethyl-N,N-diisopropylamine / ethanol / 30 °C
View Scheme
Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 5 h / 50 °C
2: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
3: triethylamine / tetrahydrofuran / 1 h / 0 °C
4: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme

5-chloropyrazolo[1,5-a]pyrimidin-3-amine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 10 °C
2: ethanol / 25 °C
3: N-ethyl-N,N-diisopropylamine / ethanol / 30 °C
View Scheme
1218935-59-1

(R)-(+)-2-(2,5-difluorophenyl)pyrrolidine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 5 h / 50 °C
2: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
3: triethylamine / tetrahydrofuran / 1 h / 0 °C
4: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme

C15H21F2NO3

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 12 h / 35 °C
1.2: 1 h
2.1: triethylamine / tetrahydrofuran / 5 h / 50 °C
3.1: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C
5.1: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme
29274-22-4

4H,5H-pyrazolo[1,5-a]pyrimidine-5-one

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: phosphorus trichloride / 6 h / 80 °C
2: nitric acid; sulfuric acid / 2 h / 0 - 5 °C
3: triethylamine / tetrahydrofuran / 5 h / 50 °C
4: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
5: triethylamine / tetrahydrofuran / 1 h / 0 °C
6: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme
29274-24-6

5-chloropyrazolo[1,5-a]pyrimidine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: nitric acid; sulfuric acid / 2 h / 0 - 5 °C
2: triethylamine / tetrahydrofuran / 5 h / 50 °C
3: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
4: triethylamine / tetrahydrofuran / 1 h / 0 °C
5: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme
1223404-90-7

(R)-5-(2-(2,5-difluorophenyl)pyrrolidin-1-yl)-3-nitropyrazolo[1,5-a]pyrimidine

1223403-58-4

(3S)-N-[5-[(2R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl]pyrazolo[1,5-a]pyrimidi n-3-yl]-3-hydroxypyrrolidine-1-carboxamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: acetic acid; hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2.5 h / 20 °C / 7600.51 Torr
2: triethylamine / tetrahydrofuran / 1 h / 0 °C
3: triethylamine / tetrahydrofuran / 6 h / 75 °C
View Scheme
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    Product name: LOXO-101(CAS:1223403-58-4) CAS No.：1223403-58-4 Molecule Formula：C21H22F2N6O2 Molecule Weight：428.44 Purity: 98.0% Package: 25kg/drum Description：Yellow powder Manufacture Standards：Enterprise Standard

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  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, s

  •  Shandong Mopai Biotechnology Co., LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-15965530500

    Address:shandong

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  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.5-1.5

    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

    KAISA GROUP INC.is the enterprise which is specialize in manfacturing and exporting avariety of Chemical in China. We have the strong economic base and comprehensive technology.We

  •  KAISA GROUP INC

    United States  |  Contact Details

    Business Type:Trading Company

    Tel:15131197030

    Address:1312 17th Street Suite 1402 Denver CO 80202

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  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    LOXO-101 is one of the most competitive products in our company. We can supply it with good quality and best price. Appearance:powder Storage:RT Package:According to the demand of customer Application:API Port:shanghai

    Nanjing Fred Technology Co.,Ltd. is a Fine Chemicals Company, specializing in research, development, manufacture and distribute raw materials for pharmaceutical, healthcare, bioc

  •  Nanjing Fred Technology Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-25-84696168

    Address:Nanjing

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  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

    SAGECHEM is a chemical R&D, manufacturing and distribution company since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and

  •  SAGECHEM LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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  • LOXO-101 1223403-58-4

  • Casno:

    1223403-58-4

    LOXO-101 1223403-58-4

    Min.Order: 100 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    Advantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit

    Jining Xinhe Pharmaceutical Co., LTD specializes in pharmaceutical apis, intermediate research and development, as well as production and sales. We have a 2000-square-meter R&D cen

  •  JINING XINHE CHEMICAL CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-15264160071

    Address:High-tech zone，Jining City Shangdong China

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  • Larotrectinib Cas no.1223403-58-4 98%

  • Casno:

    1223403-58-4

    Larotrectinib Cas no.1223403-58-4 98%

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

    Established in 2007, Win-Win chemical CO., Ltd is a privately held corporation headquartered in Wenzhou Longwan Industry Distric, dedicated to the global pharmaceutical companies a

  •  Win-Win chemical Co.Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-577-64498589

    Address:No.49 YuShi West Road, Longwan District,325000

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.0-1.0

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production in China for chemicals cus

  •  Bluecrystal chem-union

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-1895157

    Address:Liang Xi Qu

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  • Larotrectinib

  • Casno:

    1223403-58-4

    Larotrectinib

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 10.0-10.0

    Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api

    Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,an

  •  Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-317-5106598

    Address:40# Shuiyuesi Street, Cangzhou City,Hebei Province, China.

       Inquiry Now

  • LOXO-101 cas no. 1223403-58-4 API

  • Casno:

    1223403-58-4

    LOXO-101 cas no. 1223403-58-4 API

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    with high qualityAppearance:white powder Storage:Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Package:25kg/drum Application:to formulate preparations Transportation:by courier, air or sea Port:At any port fro

    Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd (JL Pharm) is established in 2012 at the beautiful West Lake – Hangzhou city, China. The company's main business includes R&D, Produ

  •  Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-571-85829053

    Address:Rm A606, Fuyi Center, jianqiao street, Jianggan Area

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  • 99% up by HPLC LOXO-101 1223403-58-4

  • Casno:

    1223403-58-4

    99% up by HPLC LOXO-101 1223403-58-4

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Why is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment .5) We can do different t

    Sinoway Industrial co., ltd. was established in 1987 in Xiamen, China, and now has been a leading group specialized in research, development, custom manufacturing and trading of ph

  •  Sinoway Industrial Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-592-583819

    Address:16/F,Huicheng Comm,Complex,No839 XiaHe Rd, Xiamen,China

       Inquiry Now

  • LOXO-101 (ARRY-470)

  • Casno:

    1223403-58-4

    LOXO-101 (ARRY-470)

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    LOXO-101, also known as ARRY-470, is an orally bioavailable, potent, ATP-competitive inhibitor of TRKA, TRKB, and TRKC. LOXO-101 has IC50 values in the low nanomolar range for inhibition of all three TRK family members in binding and cellular assay

    BOC Sciences is a brand of BOCSCI Inc. We leverage our wide spectrum of business in the fields of development, manufacturing, marketing, and distribution to help you make best-info

  •  BOC Sciences

    United States  |  Contact Details

    Business Type:Trading Company

    Tel:1-631-485-4226

    Address:Ramsey Road

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

    Antimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and

  •  Antimex Chemical Limied

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-50563169

    Address:Room1027,No.Jinyu Road,Pudong

       Inquiry Now

  • Larotrectinib（LOXO-101） CAS No.1223403-58-4

  • Casno:

    1223403-58-4

    Larotrectinib（LOXO-101） CAS No.1223403-58-4

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

    Guangdong Juda Chemical Industrial Co.,Limited is a company specializing in APIs,pharmaceutical intermediates, electronic chemicals, plant extracts,fine chemicals and cosmetics raw

  •  Guangdong Juda Chemical Industrial Co.,Limited

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 13510152023(whatsapp)

    Address:Guangzhou chemical city Tianhe District Guangzhou Guangdong China

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg，customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

  •  Wuhan Circle Star Chem-medical Technology co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

    Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketi

  •  Hangzhou ZeErRui Chemical Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-82512721

    Address:No 317,Jingling Road,Guali Town,Xiaoshan District

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:2mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port

    Shanghai Yuanye Bio-Technology Co., Ltd. is a comprehensive enterprise of life science, specializing in the research, development and sales of biochemical reagents, analytical stan

  •  Shanghai Yuanye Bio-Technology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-21-61845781

    Address:Building 6, No. 465, Changta Road,Songjiang District,Shanghai,China

       Inquiry Now

  • LOXO-101

  • Casno:

    1223403-58-4

    LOXO-101

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

    We are a team of industry experts, dedicated to delivering the best chemical solutions from quality suppliers across China. Putting our customers first, we take a holistic approach

  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-189 8945 5137

    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

       Inquiry Now

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