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Basic Information
CAS No.: 1271-03-0
Name: Cyclopentadienyl allyl palladiuM
Molecular Structure:
Molecular Structure of 1271-03-0 (Cyclopentadienyl allyl palladiuM)
Formula: C8H10 Pd
Molecular Weight: 212.587
Synonyms: Palladium,(h5-2,4-cyclopentadien-1-yl)(h3-2-propenyl)- (9CI); Palladium,allylcyclopentadienyl- (6CI); Palladium, p-allyl-p-cyclopentadienyl- (8CI); Palladium, p-allylcyclopentadienyl- (7CI); (h3-Allyl)(cyclopentadienyl)palladium;(h3-Allyl)(h5-cyclopentadienyl)palladium; (h5-h5-Cyclopentadienyl)(h3-cyclopropyl)palladium;Allyl(cyclopentadienyl)palladium; Allyl(h5-cyclopentadienyl)palladium; p-Allyl-p-cyclopentadienylpalladium; p-Cyclopentadienyl-p-allylpalladium
Density: g/cm3
Melting Point: 60-62 °C
Boiling Point: 41.5°Cat760mmHg
Flash Point: °C
PSA: 0.00000
LogP: 2.26300
Synthetic route

bis(η3-allyl-μ-chloropalladium(II))

4984-82-1

sodium cyclopentadienylide

1271-03-0

allyl(cyclopentadiene)palladium(II)

Conditions
ConditionsYield
In tetrahydrofuran; benzene at -20 - 20℃; for 1.5h; Inert atmosphere; Schlenk technique;99%

bis(η3-allyl-μ-chloropalladium(II))

sodium cyclopentadienide

1271-03-0

allyl(cyclopentadiene)palladium(II)

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere;95%
With sodium In tetrahydrofuran; benzene at -10 - -2℃; for 2h; Inert atmosphere; Glovebox;92%
In tetrahydrofuran at -60 - 20℃; for 0.75h;
In tetrahydrofuran at 0℃; Inert atmosphere;

bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]

4984-82-1

sodium cyclopentadienylide

1271-03-0

allyl(cyclopentadiene)palladium(II)

Conditions
ConditionsYield
In tetrahydrofuran at -78 - 20℃; Inert atmosphere;95%

bis(η3-allyl-μ-chloropalladium(II))

lithium cyclopentadienide

1271-03-0

allyl(cyclopentadiene)palladium(II)

Conditions
ConditionsYield
In tetrahydrofuran; toluene addn. of LiC5H5 in THF to Pd-complex in toluene, stirring (several h); solvent removal (vac.), sublimation (45°C, 1E-3 Torr);;70%

bis(η3-allyl-μ-chloropalladium(II))

1271-03-0

allyl(cyclopentadiene)palladium(II)

Conditions
ConditionsYield
With lithium cyclopentadienide In tetrahydrofuran; toluene at -30 - 20℃; for 1h; Inert atmosphere;
116-14-3

polytetrafluoroethylene

1271-03-0

allyl(cyclopentadiene)palladium(II)

65038-36-0

1,4-bis(dicyclohexylphosphino)butane

1445270-22-3

(η2-tetrafluoroethylene)Pd(1,4-bis(dicyclohexylphosphino)butane)

Conditions
ConditionsYield
In toluene at 20℃; under 760.051 Torr; for 3h; Inert atmosphere;100%
1271-03-0

allyl(cyclopentadiene)palladium(II)

119072-55-8, 7188-38-7

tert-butylisonitrile

24859-25-4

bis(tert-butyl isocyanide) palladium(0)

Conditions
ConditionsYield
In pentane Ar-atmosphere; modified procedure from J. Am. Chem. Soc. 1969, 91, 6994;addn. of excess of isocyanide to soln. of Pd-complex at -10°C, s tirring for 10 min; evapn., washing (pentane), drying (vac.);99%
In pentane (Ar); -10°C, 30 min; supernatant liq. removal, solid washing (pentane), drying (vac.);99%
1271-03-0

allyl(cyclopentadiene)palladium(II)

529-28-2

4-iodoanisol

603-35-0

triphenylphosphine

180891-47-8

(2-methoxyphenyl)Pd(P(C6H5)3)2I

Conditions
ConditionsYield
In dichloromethane Ar-atmosphere; stirring (room temp., 5 - 15 min); filtering (PTFE membrane), crystn. on concg. and hexane addn. (-30°C, overnight), filtering, drying (vac.); elem. anal.;99%
1271-03-0

allyl(cyclopentadiene)palladium(II)

598-45-8

i-propyl isocyanide

93224-59-0

Pd(CN-i-Pr)2

Conditions
ConditionsYield
In pentane Ar-atmosphere; modified procedure from J. Am. Chem. Soc. 1969, 91, 6994;addn. of excess of isocyanide to soln. of Pd-complex at -10°C, s tirring for 10 min; evapn., washing (pentane), drying (vac.);99%
1271-03-0

allyl(cyclopentadiene)palladium(II)

150043-29-1

1,1,3,3-tetramethylbutyl isocyanide

176104-88-4

Pd(CNC(CH3)2C(CH3)3)2

Conditions
ConditionsYield
In pentane Ar-atmosphere; modified procedure from J. Am. Chem. Soc. 1969, 91, 6994;addn. of excess of isocyanide to soln. of Pd-complex at -10°C, s tirring for 10 min; evapn., washing (pentane), drying (vac.);99%
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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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    China (Mainland)  |  Contact Details

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    United States  |  Contact Details

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     China (Mainland)  |  Contact Details

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    1271-03-0

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    China (Mainland)  |  Contact Details

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    1271-03-0

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Jiaojiang District, Taizhou, Zhejiang, China.

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