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1289942-66-0

Basic Information
CAS No.: 1289942-66-0
Name: N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine
Article Data: 14
Molecular Structure:
Molecular Structure of 1289942-66-0 (N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine)
Formula: C12H15FN2O3
Molecular Weight: 254.261
Synonyms: N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine;Alanine, N-[3-fluoro-4-[(MethylaMino)carbonyl]phenyl]-2-Methyl-;5.N-[3-Fluoro-4-[(MethylaMino)carbonyl]phenyl]-2-Methylalanine;N-[3-Fluoro-4-[(MethylaMino)carbonyl]phenyl]-2-Methylalanine(for EnzalutaMide)
EINECS: 807-437-3
Density: 1.286
Boiling Point: 455℃
Flash Point: 229℃
PSA: 81.92000
LogP: 2.10820
Synthetic route
292621-45-5

2-fluoro-4-bromobenzamide

propylene 2-amino-2-isobutyrate hydrochloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
With 2-acetylcyclohexanone; water; potassium carbonate; copper(l) chloride In N,N-dimethyl-formamide at 30 - 105℃; for 12h;89.1%
749927-69-3

4-bromo-2-fluoro-N-methylbenzanamide

62-57-7

2-Aminoisobutyric acid

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
With 2-acetylcyclohexanone; potassium carbonate; copper(l) chloride In N,N-dimethyl-formamide at 110℃; for 16h;88.7%
With water; potassium carbonate; L-proline; copper(l) chloride In N,N-dimethyl-formamide at 100℃; for 24h; Reagent/catalyst; Solvent; Inert atmosphere;87%
Stage #1: 4-bromo-2-fluoro-N-methylbenzanamide; 2-Aminoisobutyric acid With potassium carbonate; copper(l) chloride In water; N,N-dimethyl-formamide at 30℃;
Stage #2: With 2-acetylcyclohexanone In water; N,N-dimethyl-formamide at 105℃; Inert atmosphere;
Stage #3: With citric acid In Isopropyl acetate; water pH=4;
75.4%
749927-69-3

4-bromo-2-fluoro-N-methylbenzanamide

15028-41-8

methyl 2-aminoisobutyrate hydrochloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
With 2-acetylcyclohexanone; water; potassium carbonate; copper(l) chloride In N,N-dimethyl-formamide at 30 - 105℃; for 12h;87.3%
292621-45-5

2-fluoro-4-bromobenzamide

60421-20-7

benzyl 2-amino-2-methylpropionate hydrochloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
With copper(l) iodide; 2-acetylcyclohexanone; water; potassium carbonate In dimethyl sulfoxide at 40 - 110℃; for 10h;83.6%
915087-25-1

2-fluoro-N-methyl-4-amino-benzamide

2052-01-9

2-bromo-2-methylpropionic acid

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 72h;76%
With triethylamine In dichloromethane at 20 - 30℃; for 15h; Inert atmosphere;12 g
With triethylamine In dichloromethane at 20 - 30℃; for 15h; Inert atmosphere;
2052-01-9

2-bromo-2-methylpropionic acid

4-amino-2-fluoro-N-methylbenzamide hydrochloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
Stage #1: 4-amino-2-fluoro-N-methylbenzamide hydrochloride With triethylamine In N,N-dimethyl acetamide at 70℃; for 1h;
Stage #2: 2-bromo-2-methylpropionic acid In N,N-dimethyl acetamide at 100℃; for 1.66667h;
53%
112704-79-7

2-fluoro-4-bromobenzoic acid

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: thionyl chloride / N,N-dimethyl-formamide; Isopropyl acetate / 4.58 h / 21 - 72 °C / Inert atmosphere; Industry scale
2.1: water; Isopropyl acetate / 1.08 h / 2 - 35 °C / Inert atmosphere; Industry scale
3.1: potassium carbonate / copper(l) chloride / N,N-dimethyl-formamide; water / 30 °C
3.2: 105 °C / Inert atmosphere
3.3: pH 4
View Scheme
Multi-step reaction with 3 steps
1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 10 - 30 °C
2.1: water; tert-butyl methyl ether / 10 - 30 °C / pH 8 - 9
3.1: potassium carbonate / N,N-dimethyl-formamide; 1,4-dioxane; water / 0.33 h / Inert atmosphere
3.2: 24.33 h / Inert atmosphere; Reflux
View Scheme
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide; thionyl chloride / ethyl acetate / 4 h / 20 °C / Inert atmosphere; Reflux
2: ethyl acetate / 0.25 h / 30 - 35 °C
3: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere
View Scheme
151982-51-3

4-bromo-2-fluorobenzoyl chloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: water; Isopropyl acetate / 1.08 h / 2 - 35 °C / Inert atmosphere; Industry scale
2.1: potassium carbonate / copper(l) chloride / N,N-dimethyl-formamide; water / 30 °C
2.2: 105 °C / Inert atmosphere
2.3: pH 4
View Scheme
Multi-step reaction with 2 steps
1: ethyl acetate / 0.25 h / 30 - 35 °C
2: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: toluene; N,N-dimethyl-formamide / 1 h / 10 - 15 °C
2.1: copper(l) chloride; N,N-dimethyl-aniline / N,N-dimethyl-formamide / 75 - 80 °C / Inert atmosphere
2.2: 75 - 80 °C / Inert atmosphere
2.3: 0.25 h / Inert atmosphere
View Scheme
403-24-7

2-fluoro-4-nitrobenzoic acid

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: N,N-dimethyl-formamide; thionyl chloride / Isopropyl acetate / 60 °C / Inert atmosphere
2.1: Isopropyl acetate / 5 h / Inert atmosphere
3.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 50 °C / 4500.45 Torr / Autoclave
3.2: Heating
4.1: triethylamine / N,N-dimethyl acetamide / 1 h / 70 °C
4.2: 1.67 h / 100 °C
View Scheme
403-23-6

2-fluoro-4-nitrobenzoyl chloride

1289942-66-0

2-((3-fluoro-4-(methylcarbamoyl)phenyl)amino)-2-methyl propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: Isopropyl acetate / 5 h / Inert atmosphere
2.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 50 °C / 4500.45 Torr / Autoclave
2.2: Heating
3.1: triethylamine / N,N-dimethyl acetamide / 1 h / 70 °C
3.2: 1.67 h / 100 °C
View Scheme
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    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine CAS No.:1289942-66-0 Name: N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine Molecular Structure Molecular Formula: C12H15FN2O3

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    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine CAS: 1289942-66-0 Specification Name: N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine Molecular Structure Molecular Formula: C12H15FN2O3 Molecular Weight: 254.26

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    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Our product has a very high quality and now we are exporting to customers overseas with very positive feedback. With best price, quality and service from Nanjing Sunny, we are confident to set up a very nice cooperation with customers all over the w

    Welcome to Sunny Pharmatech! Nanjing Sunny pharmatech Co., Ltd is a manufacturer and supplier of raw materials and ingredients for food and healthy supplement products, intermediat

  •  NANJING SUNNY PHARMATECH CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-13814179829

    Address:No. 1704 SHUANGLONOG AVENUE, NANJING, CHINA

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  • N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

    SAGECHEM is a chemical R&D, manufacturing and distribution company since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and

  •  SAGECHEM LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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  • N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

    GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production. Currently our major business is: 1.Con

  •  Golden Pharma Co., Limited

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:18958062155

    Address:1

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  • N-[3-Fluoro-4-[carbonyl]phenyl]-2-methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[carbonyl]phenyl]-2-methylalanine

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 9.0-9.0

    Company name: Falcon Life Sciences Pvt. Ltd. was established in 2015, specializing in the sales and production of intermediates and raw materials. We are committed to providing customers with quality products and excellent service. We firmly believ

    Falcon Life Sciences Pvt. Ltd. based in Xi'an, China is trading in healthcare products. We export health care products and also provide sourcing services to our overseas buyers.

  •  Falcon Life Sciences Pvt. Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8613201721613

    Address:Da Qing Lu, Huawei Yun

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  • N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

  •  GIHI CHEMICALS CO.,LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86217390

    Address:No.567 Dengcai Street,Sandun,Westlake District,Hangzhou310030,Zhejiang,China.

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  • N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine CAS 1289942-66-0

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine CAS 1289942-66-0

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

    Wuxi TAA Chemical Industry Co.,Ltd., established in 2010, is a key chemical manufacturer and supplier in China. In 2010, three young chemists from a local large state-owned chemi

  •  Wuxi TAA Chemical Industry Co.,LTD.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:18168326835

    Address:2202 Scientific Research Business Center, Lihu Road, Wuxi 214128 China

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  • N-[3-Fluoro-4-[(Methylamino)Carbonyl]Phenyl]-2-Methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(Methylamino)Carbonyl]Phenyl]-2-Methylalanine

    Min.Order: 100 Gram

    FOB Price:  USD $ 0.0-0.0

    Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

    Jinhua huayi chemical co., ltd. has own manufacturers which focus on production of organic specialty products,Pharmaceuticals and its intermediates,fine chemcals of high purity.The

  •  JINHUA HUAYI CHEMICAL CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-579-82660891

    Address:47-204 No.288, Shida St., Wuchem Dist., Jinhua,Zhejiang, 321004 China

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  • N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

  • Casno:

    1289942-66-0

    N-[3-Fluoro-4-[(methylamino)carbonyl]phenyl]-2-methylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    The factory directly supplies and ships products with guaranteed quality Package:It is packed with polythene bag as inner layer, and a compound plastic woven bag as outer layer. The net weight of each bag is 86kg. Application:Used in multiple fields

    Hangzhou Dingyan Chem Co., LTD. is located in the beautiful tourist city of hangzhou, is a comprehensive chemical enterprice which doing import and export business by its own comp

  •  Hangzhou Dingyan Chem Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-87157530-8003

    Address:RM.1118,NO.1 Building, Baiyun Tower,Jianggan Area, Hangzhou city, China,310004

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