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131826-11-4

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Basic Information
CAS No.: 131826-11-4
Name: 3-Isobutylaniline
Molecular Structure:
Molecular Structure of 131826-11-4 (3-Isobutylaniline)
Formula: C10H15N
Molecular Weight: 149.236
Synonyms: 3-isobutylphenylamine;3-Isobutylaniline;3-sek.Butyl-anilin;
Density: 0.944±0.06 g/cm3(Predicted)
Boiling Point: 245.7±9.0 °C(Predicted)
PSA: 26.02000
LogP: 3.04850
Synthetic route
6026-73-9

1-(2-methyl-1-propenyl)-3-nitrobenzene

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
With sodium hypophosphite monohydrate; palladium on activated charcoal; sodium carbonate In acetic acid butyl ester; water for 3h; Reagent/catalyst; Reflux;93%
With hydrogenchloride; palladium on activated carbon In methanol; sodium hydrogencarbonate; ethyl acetate

C16H31NSi2

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
Inert atmosphere;
121-73-3

3-Chloronitrobenzene

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: (η3-allyl)(N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)chloropalladium(II); sodium carbonate / acetic acid butyl ester / 5 h / 160 °C / Autoclave
2: sodium hypophosphite monohydrate; palladium on activated charcoal; sodium carbonate / acetic acid butyl ester; water / 3 h / Reflux
View Scheme
585-79-5

3-Bromonitrobenzene

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate; sodium carbonate / acetic acid butyl ester / 10 h / 140 °C / Autoclave
2: sodium hypophosphite monohydrate; palladium on activated charcoal; sodium carbonate / acetic acid butyl ester; water / 3 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene; sodium carbonate / acetic acid butyl ester / 5 h / 140 °C / Autoclave
2: sodium hypophosphite monohydrate; palladium on activated charcoal; sodium carbonate / acetic acid butyl ester; water / 3 h / Reflux
View Scheme
42528-67-6

m-amino isobutyrophenone

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
With hydrazine hydrate; potassium hydroxide In diethylene glycol at 105 - 180℃; for 8h; Temperature;
591-19-5

3-bromoaniline

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,4-dioxane / 12 h / 100 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / 1 h / 25 °C / 2585.81 Torr
View Scheme
153624-73-8

3-(2-methylprop-1-en-1-yl)aniline

131826-11-4

3-isobutylaniline

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen at 25℃; under 2585.81 Torr; for 1h;
677-69-0

perfluoroisopropyl iodide

131826-11-4

3-isobutylaniline

870786-82-6

3-isobutyl-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]aniline

Conditions
ConditionsYield
With sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In tert-butyl methyl ether; water at 20℃;60%
With sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In tert-butyl methyl ether; water at 20℃;47%
aqueous sodium nitrite

aqueous sodium nitrite

131826-11-4

3-isobutylaniline

139155-55-8

1-bromo-3-isobutylbenzene

Conditions
ConditionsYield
With copper(I) bromide In hydrogen bromide
131826-11-4

3-isobutylaniline

870786-83-7

3-isobutyl-4-[1-methoxy-2,2,2-trifluoro-1-(trifluoromethyl)ethyl]aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium dithionite / water; tert-butyl methyl ether / 20 °C
2: methanol / 5 h / Reflux
View Scheme
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    CAS: 131826-11-4 MF: C10H15N MW: 149.2328 EINECS: Properties Boiling point: 245.7±9.0 °C(Predicted) Density 0.944±0.06 g/cm3(P

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