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1484-04-4

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Basic Information
CAS No.: 1484-04-4
Name: 1-(9-ETHYL-9H-CARBAZOL-3-YL)ETHANONE
Article Data: 25
Molecular Structure:
Molecular Structure of 1484-04-4 (1-(9-ETHYL-9H-CARBAZOL-3-YL)ETHANONE)
Formula: C16H15NO
Molecular Weight: 237.301
Synonyms: 1-(9-ethylcarbazol-3-yl)ethanone;
Density: 1.12g/cm3
Melting Point: 115 °C
Boiling Point: 353.5oC at 760 mmHg
Flash Point: 167.6oC
PSA: 22.00000
LogP: 4.01700
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Synthetic route
86-28-2

N-ethylcarbazole

75-36-5

acetyl chloride

1484-04-4

N-ethyl-3-acetylcarbazole

Conditions
ConditionsYield
With bismuth(III) chloride In dichloromethane at 20℃; Friedel Crafts acylation;81%
With zinc(II) chloride In dichloromethane at 20℃; for 6h; Friedel Crafts acylation;80%
With zinc(II) chloride Friedel-Crafts Acylation;
86-28-2

N-ethylcarbazole

108-24-7

acetic anhydride

1484-04-4

N-ethyl-3-acetylcarbazole

Conditions
ConditionsYield
Stage #1: N-ethylcarbazole; acetic anhydride With boron trifluoride diethyl etherate at 20℃; for 4h;
Stage #2: With hydrogenchloride; water		80.4%
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation;70%
With aluminum (III) chloride In dichloromethane at 20℃; for 4h;70.47%
86-28-2

N-ethylcarbazole

506-96-7

Acetyl bromide

1484-04-4

N-ethyl-3-acetylcarbazole

Conditions
ConditionsYield
Stage #1: N-ethylcarbazole; Acetyl bromide With tin(IV) chloride In dichloromethane at 20℃; for 24h;
Stage #2: With hydrogenchloride In dichloromethane; water Cooling with ice;		80%
With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 5h;74%
With aluminum (III) chloride In 1,2-dichloro-ethane74%
86-28-2

N-ethylcarbazole

137131-39-6

C10H12N2O4

A

1484-04-4

N-ethyl-3-acetylcarbazole

B

1355624-73-5

ethyl 5-(1-cyano-2-ethoxy-2-oxoethylidene)prolinate

C

ethyl 5-[2-amino-1-(ethoxycarbonyl)-2-oxoethylidene]prolinate

D

1355624-71-3

ethyl 5-[1-cyano-2-(9-ethyl-9H-carbazol-3-yl)-2-oxoethylidene]prolinate

Conditions
ConditionsYield
With Eaton′s Reagent at 60℃; for 30h; Inert atmosphere;A 1%
B 20%
C 9%
D 40%
...Expand
86-28-2

N-ethylcarbazole

75-36-5

acetyl chloride

A

1484-04-4

N-ethyl-3-acetylcarbazole

B

1483-97-2

1,1′-(9-ethyl-9H-carbazole-3,6-diyl)diethanone

Conditions
ConditionsYield
With carbon disulfide; aluminium trichloride
...Expand
86-74-8

9H-carbazole

75-36-5

acetyl chloride

1484-04-4

N-ethyl-3-acetylcarbazole

Conditions
ConditionsYield
With aluminium trichloride
86-28-2

N-ethylcarbazole

108-24-7

acetic anhydride

A

1484-04-4

N-ethyl-3-acetylcarbazole

B

1483-97-2

1,1′-(9-ethyl-9H-carbazole-3,6-diyl)diethanone

Conditions
ConditionsYield
With aluminum (III) chloride Friedel Crafts acylation;
...Expand
86-74-8

9H-carbazole

1484-04-4

N-ethyl-3-acetylcarbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; acetone / 12 h / Reflux
2.1: tin(IV) chloride / dichloromethane / 24 h / 20 °C
2.2: Cooling with ice
View Scheme
Multi-step reaction with 2 steps
1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.67 h / 20 °C
1.2: 10 h / 20 °C
2.1: boron trifluoride diethyl etherate / 4 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate / acetone / 20 °C
2: zinc(II) chloride / dichloromethane / 24 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h
1.2: 2 h / 20 °C
2.1: aluminum (III) chloride / dichloromethane / 0.5 h / 20 °C
2.2: 6 h / 0 - 20 °C
View Scheme
2002-03-1

2-amino-5-phenyl-1,3,4-thiadiazole

1484-04-4

N-ethyl-3-acetylcarbazole

C24H20N4S

Conditions
ConditionsYield
With choline chloride; oxalic acid at 70℃;95.1%
1484-04-4

N-ethyl-3-acetylcarbazole

33621-62-4

2-amino-5-(4'-bromophenyl)-1,3,4-oxadiazole

C24H19BrN4O

Conditions
ConditionsYield
With choline chloride; oxalic acid at 70℃;88.2%
With toluene-4-sulfonic acid at 20℃; for 0.25h; Reagent/catalyst; Schiff Reaction;81.6%
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