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CAS No.: | 163520-33-0 | ||||||||||
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Name: | ISOXADIFEN-ETHYL | ||||||||||
Article Data: | 7 | ||||||||||
Molecular Structure: | |||||||||||
Formula: | C18H17 N O3 | ||||||||||
Molecular Weight: | 295.338 | ||||||||||
Synonyms: | AE-F122006; HOE 122006; Isoxadifen ethyl ester; Isoxadifen-ethyl | ||||||||||
EINECS: | 443-870-0 | ||||||||||
Density: | 1.15g/cm3 | ||||||||||
Melting Point: | 87-88℃ (ethyl ether ) | ||||||||||
Boiling Point: | 407.7°Cat760mmHg | ||||||||||
Flash Point: | 166.8°C | ||||||||||
Solubility: | 1.06mg/L at 20℃ | ||||||||||
Hazard Symbols: | |||||||||||
Risk Codes: | 22-43-50 | ||||||||||
Safety: |
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PSA: | 47.89000 | ||||||||||
LogP: | 2.70520 |
ethyl 2,2-diphenylcyclopropane-1-carboxylate
isoxadifen-ethyl
Conditions | Yield |
---|---|
With trifluoroacetic acid; sodium nitrite at 18 - 40℃; for 0.5h; Reagent/catalyst; | 89% |
Conditions | Yield |
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With 1,4-diaza-bicyclo[2.2.2]octane In ethanol at 80℃; for 120h; | 75% |
Conditions | Yield |
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With tert.-butylnitrite; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium hydrogencarbonate; zinc dibromide In tert-butyl methyl ether at 20℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 67% |
Conditions | Yield |
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With sodium hydrogencarbonate In isopropyl alcohol at 40℃; for 24h; |
benzophenone hydrazone
isoxadifen-ethyl
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: mercury(II) oxide / Petroleum ether / 16 h / 20 °C 2: Petroleum ether / 0.17 h / 50 °C 3: sodium nitrite; trifluoroacetic acid / 0.5 h / 18 - 40 °C View Scheme |
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 2h; | 12.7 g |
1,1-Diphenylethylene
ethyl 2-chloro-2-(hydroxyimino)acetate
isoxadifen-ethyl
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 25 - 30℃; Temperature; | 13 g |
isoxadifen-ethyl
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol; dichloromethane at 20℃; for 6h; | 92% |
With sodium tetrahydroborate In methanol for 1h; Heating; |
isoxadifen-ethyl
Conditions | Yield |
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Multi-step reaction with 2 steps 1: NaBH4 / methanol / 1 h / Heating 2: SOCl2 / benzene / 1 h / Heating View Scheme |
isoxadifen-ethyl
C-(5,5-diphenyl-4,5-dihydro-isoxazol-3-yl)-methylamine
Conditions | Yield |
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Multi-step reaction with 4 steps 1: NaBH4 / methanol / 1 h / Heating 2: SOCl2 / benzene / 1 h / Heating 3: dimethylformamide / 20 °C 4: NH2NH2 / methanol / 2 h / 60 °C View Scheme |