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1806-29-7

Basic Information
CAS No.: 1806-29-7
Name: 2,2'-Biphenol
Article Data: 66
Cas Database
Molecular Structure:
Molecular Structure of 1806-29-7 (2,2'-Biphenol)
Formula: C12H10O2
Molecular Weight: 186.21
Synonyms: 2,2'-Biphenyldiol(8CI);1,1'-Bi-2-phenol;2,2'-Dihydroxy-1,1'-biphenyl;2,2'-Dihydroxybiphenyl;2,2'-Dihydroxydiphenyl;2'-Hydroxy-1,1'-biphenyl-2-ol;NSC 37068;o,o'-Biphenol;o,o'-Dihydroxybiphenyl;o,o'-Diphenol;[1,1'-Biphenyl]-2,2'-diol;
EINECS: 217-303-0
Density: 1.228 g/cm3
Melting Point: 108-110 °C
Boiling Point: 314.999 °C at 760 mmHg
Flash Point: 160.803 °C
Solubility: insoluble in water
Appearance: Beige to greyish-beige powder
Hazard Symbols: HarmfulXn,IrritantXi
Risk Codes: 36/37/38-41-22
Safety: 26-39-36/37/39
Transport Information: N/A
PSA: 40.46000
LogP: 2.76480
Synthetic route
1227735-80-9

6,6-diisopropyldibenzo[d,f][1,3,2]dioxasilepine

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;100%
6390-69-8

3,3',5,5'-tetra(tert-butyl)biphenyl-2,2'-diol

A

1806-29-7

2,2'-dihydroxybiphenyl

B

98-51-1

4-tert-butyltoluene

Conditions
ConditionsYield
With Nafion-H; toluene for 2h; Heating;A 98%
B 98 % Chromat.
6390-69-8

3,3',5,5'-tetra(tert-butyl)biphenyl-2,2'-diol

108-88-3

toluene

A

1806-29-7

2,2'-dihydroxybiphenyl

B

98-51-1

4-tert-butyltoluene

Conditions
ConditionsYield
With Nafion-H for 2h; Heating;A 98%
B 98 % Chromat.
533-58-4

2-Iodophenol

89466-08-0

2-hydroxyphenyl boronic acid

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With palladium 10% on activated carbon; potassium carbonate In water at 80℃; for 2.5h; Suzuki-Miyaura Coupling; Inert atmosphere;98%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In N,N-dimethyl-formamide at 160℃; for 0.5h; Suzuki Coupling; Microwave irradiation;
With palladium on activated charcoal; potassium carbonate In water at 80℃; Suzuki Coupling;

2,2'-dihydroxy-4,4'-biphenyldisulfonic acid

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With sulfuric acid at 100℃; for 2h;98%
4877-93-4

2,2'-Dimethoxybiphenyl

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With aluminium trichloride In ethanethiol for 0.5h; Ambient temperature;97.5%
With aluminium trichloride In ethanethiol for 0.5h; Ambient temperature;97.5%
1196786-63-6

C30H50O2Si2

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With potassium fluoride In Tetraethylene glycol at 20℃; for 0.5h; Inert atmosphere;96%
With potassium fluoride; Tetraethylene glycol at 20℃; for 0.5h;96%
1114567-49-5

2,2'-biphenol bis(tert-butyldimethylsilyl) ether

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With lithium acetate In water; N,N-dimethyl-formamide at 70℃; for 6h; Inert atmosphere;92%
220-11-1

dibenzo[d,f][1,3]dioxepin

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With hydrogenchloride In ethanol; water at 50℃;92%
With hydrogenchloride; water In ethanol at 50℃;92%
95-57-8

2-monochlorophenol

1806-29-7

2,2'-dihydroxybiphenyl

Conditions
ConditionsYield
With potassium carbonate In ethanol; water at 20℃; for 12h; Ullmann Condensation;92%
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  • biphenol CAS:1806-29-7

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    1806-29-7

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    biphenol CAS:1806-29-7

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    1806-29-7

    2,2'-Biphenol

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    2,2'-Biphenol Basic information Product Name: 2,2'-Biphenol Synonyms: Orthodiphenol;2,2'-Biphenol,99%;2,2'-Dihydroxybiphenyl,99%;2,2’-Biphenol (2,2’-Dihydroxybiphenyl);2,2'-dihydroxybipphenol;2,2zzhlxy-Biphenol;

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  • 2,2'-BiphenolCAS NO.: 1806-29-7

  • Casno:

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    2,2'-BiphenolCAS NO.: 1806-29-7

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Chemistry

Molecular Structure of 2,2'-Biphenyldiol (CAS NO.1806-29-7):

IUPAC Name: 2-(2-Hydroxyphenyl)phenol
Canonical SMILES: C1=CC=C(C(=C1)C2=CC=CC=C2O)O
InChI: InChI=1S/C12H10O2/c13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)14/h1-8,13-14H
InChIKey: IMHDGJOMLMDPJN-UHFFFAOYSA-N
Molecular Weight: 186.2066 [g/mol]
Molecular Formula: C12H10O2
XLogP3: 3
H-Bond Donor: 2
H-Bond Acceptor: 2 
EINECS: 217-303-0 
Water Solubility: insoluble
Appearance: Beige to greyish-beige powder
Melting Point: 108-110 °C
Index of Refraction: 1.639
Molar Refractivity: 54.6 cm3
Molar Volume: 151.5 cm3
Surface Tension: 53.8 dyne/cm
Density: 1.228 g/cm3
Flash Point: 160.8 °C
Enthalpy of Vaporization: 57.84 kJ/mol
Boiling Point: 315 °C at 760 mmHg
Vapour Pressure: 0.000243 mmHg at 25 °C
Classification Code: Mutation data
Product Categories: Aromatic Phenols; Biphenyls (for High-Performance Polymer Research); Color Former & Related Compounds; Developer; Functional Materials; Reagent for High-Performance Polymer Research

Uses

 2,2'-Biphenyldiol (CAS NO.1806-29-7) is used as pharmaceutical intermediates.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 150mg/kg (150mg/kg)   National Technical Information Service. Vol. AD691-490,
mouse LD50 intravenous 56mg/kg (56mg/kg)   U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#07870,

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal and intravenous routes. Human mutation data reported. When heated to decomposition it emits acrid smoke and irritating fumes.

Hazard Codes :IrritantXi,HarmfulXn
Risk Statements: 36/37/38-41-22
R22: 2,2'-Biphenyldiol (CAS NO.1806-29-7) is harmful if swallowed. 
R41:Risk of serious damage to the eyes. 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
WGK Germany: 2
RTECS: DV4200000
F: 8-9-23

Specification

 2,2'-Biphenyldiol (CAS NO.1806-29-7), its Synonyms are 2,2'-Biphenol ; 2,2'-Dihydroxybiphenyl ; 2,2'-Dihydroxydiphenyl ; O,O'-Biphenol ; o,o'-Biphenol ; o,o'-Dihydroxybiphenyl ; o,o'-Diphenol ; o-Dihydroxydiphenyl ; (1,1'-Biphenyl)-2,2'-diol ; Biphenyl-2,2'-diol .