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19853-09-9

Basic Information
CAS No.: 19853-09-9
Name: 2-PHENYLBENZYL BROMIDE
Article Data: 28
Molecular Structure:
Molecular Structure of 19853-09-9 (2-PHENYLBENZYL BROMIDE)
Formula: C13H11 Br
Molecular Weight: 247.134
Synonyms: Biphenyl,2-(bromomethyl)- (6CI,8CI);1-Bromomethyl-2-phenylbenzene; 2-(Bromomethyl)biphenyl;2-Bromomethyl-1,1'-biphenyl; 2-Phenylbenzyl bromide; Biphenyl-2-ylmethylbromide; NSC 97772; o-Phenylbenzyl bromide
Density: 1.341g/cm3
Melting Point: 45-46 °C
Boiling Point: 374.7°Cat760mmHg
Flash Point: 169°C
Hazard Symbols:
Risk Codes: 34
Safety:
Hazard Codes C
Risk Statements 34
Safety Statements 26-27-28-36/37/39
RIDADR UN 3265 8/PG 2
WGK Germany 3
HazardClass 8
PackingGroup III
PSA: 0.00000
LogP: 4.24850
Synthetic route
2928-43-0

2-biphenylmethanol

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
With hydrogen bromide for 21h; Heating;96.6%
With carbon tetrabromide; triphenylphosphine In acetonitrile at 0 - 20℃; for 0.5h;55%
With phosphorus tribromide
643-58-3

2-methylbiphenyl

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
With tert.-butylhydroperoxide; N-Bromosuccinimide In cyclohexane at 50℃; for 4h; Reagent/catalyst; Temperature;96.5%
With tert.-butylhydroperoxide; N-Bromosuccinimide In cyclohexane at 42 - 45℃; for 2h; Green chemistry;91.2%
With N-Bromosuccinimide In tetrachloromethane for 3h; Irradiation;85%

sodium metabisulfite

Na2 S2 O5

Na2 S2 O5

643-58-3

2-methylbiphenyl

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
With N-Bromosuccinimide In nitrogen; water; chlorobenzene86%
98-80-6

phenylboronic acid

3433-80-5

1-Bromo-2-bromomethyl-benzene

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium carbonate In 1,4-dioxane at 100℃; for 3h;79%
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium carbonate In 1,4-dioxane at 100℃; for 3h; Suzuki Coupling;79%
2928-43-0

2-biphenylmethanol

18982-54-2

o-bromobenzyl alcohol

A

19853-09-9

2-phenylbenzyl bromide

B

3433-80-5

1-Bromo-2-bromomethyl-benzene

Conditions
ConditionsYield
With bromine; triphenylphosphine In dichloromethane at -78 - 20℃; for 18h; Inert atmosphere;A 75%
B 10%
2928-43-0

2-biphenylmethanol

A

19853-09-9

2-phenylbenzyl bromide

B

α,α'-dibromo-2,2'-diphenyl-bibenzyl

Conditions
ConditionsYield
With hydrogen bromide
16605-99-5

biphenyl-2-carboxylic acid methyl ester

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98.7 percent / LAH / diethyl ether
2: 96.6 percent / 48percent HBr / 21 h / Heating
View Scheme
24973-49-7

biphenyl-2-carbonitrile

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: nickel / 120 - 130 °C / 11400 - 15200 Torr / Hydrogenation
2: sodium nitrite; acetic acid
3: hydrobromic acid / 100 °C
View Scheme
1924-77-2

2-phenylbenzylamine

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium nitrite; acetic acid
2: hydrobromic acid / 100 °C
View Scheme
Multi-step reaction with 2 steps
1: NaNO2; aqueous acetic acid
2: PBr3
View Scheme
23533-35-9

biphenyl-2-ylmagnesium iodide

19853-09-9

2-phenylbenzyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether; benzene
2: aqueous HBr
View Scheme
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