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Basic Information
| CAS No.: | 2016-57-1 |
|---|---|
| Name: | Decylamine |
| Molecular Structure: | |
|
|
|
| Formula: | C10H23N |
| Molecular Weight: | 157.299 |
| Synonyms: | Decylamine(6CI,8CI);1-Aminodecane;Decanamine;Kemamine P 190D;Monodecylamine;n-Decylamine; |
| EINECS: | 217-957-7 |
| Density: | 0.797 g/cm3 |
| Melting Point: | 12-14 °C(lit.) |
| Boiling Point: | 221.403 °C at 760 mmHg |
| Flash Point: | 85.556 °C |
| Appearance: | colourless liquid |
| Hazard Symbols: |
 T
|
| Risk Codes: | 20/22-24-34 |
| Safety: | 26-36/37/39-45 |
| Transport Information: | UN 2922 8/PG 3 |
| PSA: | 26.02000 |
| LogP: | 3.78610 |
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Synthetic route
- 2016-57-1
1-aminodecane
Conditions
| Conditions | Yield |
|---|---|
| With palladium 10% on activated carbon; hydrogen In methanol at 100℃; under 37503.8 Torr; Reagent/catalyst; Flow reactor; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In water at 100℃; for 8h; pH=5.5; | 97% |
| With hydrogen; acetic acid at 20℃; under 6080.41 Torr; for 6h; Catalytic behavior; Temperature; Pressure; Sealed tube; chemoselective reaction; | 90% |
| With ammonia; hydrogen In water; isopropyl alcohol at 80℃; under 15001.5 Torr; for 24h; Autoclave; | 88% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen at 100℃; under 7500.75 Torr; for 12h; Sealed tube; Autoclave; | 97% |
- 62103-13-3
1-azidodecane
- 2016-57-1
1-aminodecane
Conditions
| Conditions | Yield |
|---|---|
| With magnesium In methanol for 0.25h; | 95% |
| With hydrogenchloride; indium In tetrahydrofuran at 20℃; for 2h; | 92% |
| With tin(ll) chloride; aluminium trichloride In methanol for 1h; Ambient temperature; | 88% |
- 69420-13-9
decyl-N,N-diallylamine
- 2016-57-1
1-aminodecane
Conditions
| Conditions | Yield |
|---|---|
| With Wilkinson's catalyst In water; acetonitrile for 2h; Heating; | 90% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; sodium hydroxide In tetrahydrofuran; water NaN3 was added to a THF soln. of trialkylborane followed by 10% aq. HCl, mixt. was gently relfuxed overnight; dild. with aq. HCl, extd. with ether, aq. layer was made basic (aq. NaOH) and ext. with ether, ether exts. were dried over KOH, filtered, evapd.; | 80% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; titanium tetrachloride In 1,2-dimethoxyethane for 14h; Ambient temperature; | 75% |
| With sodium (tert-butylamino)trihydroborate In tetrahydrofuran at 66℃; for 120h; further reducing agent: sodium (dimethylamino)trihydroborat (NaDMAB); | 46% |
| With copper oxide-chromium oxide; ammonia at 350℃; under 294203 Torr; Hydrogenation; | |
| With ethandithiol; sodium tetrahydroborate | |
| With 1,10-Phenanthroline; diethoxymethylane; iron(II) acetate In toluene at 100℃; for 28h; Inert atmosphere; chemoselective reaction; | 49 %Chromat. |
- 2016-57-1
1-aminodecane
Conditions
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; sodium hypochlorite In water 1.) 0 deg C, 5-10 min, 2.) 0 deg C -> room temperature; | 74% |
- 67-56-1
methanol
- 16423-52-2
N-decyl-N-ethylpropanamide
A
- 2016-57-1
1-aminodecane
B
- 79-20-9
acetic acid methyl ester
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: N-decyl-N-ethylpropanamide With triphenyl phosphite; chlorine; triethylamine In dichloromethane at -30℃; Stage #2: methanol In dichloromethane at -30 - 20℃; Stage #3: With water | A 72% B n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With [2,2]bipyridinyl; C24H26FeN6(2+)*2ClO4(1-); bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 80℃; for 2h; Catalytic behavior; Reagent/catalyst; Glovebox; Inert atmosphere; Molecular sieve; chemoselective reaction; | A 5% B 66% |
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Decylamine
Chemistry
MF: C10H23N
MW: 157.3
EINECS: 217-957-7
Mol File: 2016-57-1.mol
mp: 12-14 °C(lit.)
bp: 216-218 °C(lit.)
density: 0.787 g/mL at 25 °C(lit.)
refractive index: n20/D 1.436(lit.)
Fp: 186 °F
CAS DataBase Reference: 2016-57-1(CAS DataBase Reference)
NIST Chemistry Reference: 2016-57-1(NIST)
The structure of Decylamine is:
Toxicity Data With Reference
| 1. | skn-rbt 100 µg/24H open | AIHAAP American Industrial Hygiene Association Journal. 23 (1962),95. | ||
| 2. | orl-rat LD50:280 mg/kg | AIHAAP American Industrial Hygiene Association Journal. 23 (1962),95. | ||
| 3. | skn-rbt LD50:350 mg/kg | AIHAAP American Industrial Hygiene Association Journal. 23 (1962),95. | ||
| 4. | ipr-mus LD50:71 mg/kg | EJMCA5 European Journal of Medicinal Chemistry. Chimie Therapeutique. 26 (1991),517. |
Consensus Reports
1-DECANEAMINE is reported in EPA TSCA Inventory.
Safety Profile
Hazard Codes: T
Risk Statements: 22-24-34-20/22
Safety Statements: 26-36/37/39-45
RIDADR: UN 2922 8/PG 3
WGK Germany: 2
RTECS： HD6475000
F： 10-34
HazardClass： 8
PackingGroup： III
Poison by ingestion and skin contact. A skin irritant. Flammable when exposed to heat or flame; can react with oxidizing materials. To fight fire, use alcohol foam, foam, dry chemical. When heated to decomposition it emits toxic fumes of NOx.
Risk Statements: 22-24-34-20/22
Safety Statements: 26-36/37/39-45
RIDADR: UN 2922 8/PG 3
WGK Germany: 2
RTECS： HD6475000
F： 10-34
HazardClass： 8
PackingGroup： III
Poison by ingestion and skin contact. A skin irritant. Flammable when exposed to heat or flame; can react with oxidizing materials. To fight fire, use alcohol foam, foam, dry chemical. When heated to decomposition it emits toxic fumes of NOx.
Standards and Recommendations
DOT Classification: 8; Label: Corrosive, Flammable Liquid (UN 2734); DOT Class: 3; Label: Flammable Liquid, Corrosive (UN 2733)
Specification
Handling and Storage of Decylamine
Storage：Keep away from heat, sparks, and flame. Keep away from sources of ignition. Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.
Handling：Wash thoroughly after handling. Use only in a well ventilated area. Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Empty containers retain product residue, (liquid and/or vapor), and can be dangerous. Keep container tightly closed. Avoid contact with heat, sparks and flame. Do not ingest or inhale. Discard contaminated shoes. Do not pressurize, cut, weld, braze, solder, drill, grind, or expose empty containers to heat, sparks or open flames.
Storage：Keep away from heat, sparks, and flame. Keep away from sources of ignition. Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.
Handling：Wash thoroughly after handling. Use only in a well ventilated area. Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Empty containers retain product residue, (liquid and/or vapor), and can be dangerous. Keep container tightly closed. Avoid contact with heat, sparks and flame. Do not ingest or inhale. Discard contaminated shoes. Do not pressurize, cut, weld, braze, solder, drill, grind, or expose empty containers to heat, sparks or open flames.