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CAS No.: | 2187-88-4 |
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Name: | 1,4,5,8-Naphthalenetetramine |
Article Data: | 2 |
Molecular Structure: | |
Formula: | C10H12N4 |
Molecular Weight: | 188.232 |
Synonyms: | 1,4,5,8-Naphthalenetetramine;1,4,5,8-tetra-aminonaphthalene; |
PSA: | 104.08000 |
LogP: | 3.49340 |
Conditions | Yield |
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With tin(ll) chloride In hydrogenchloride; ethanol at 40℃; for 2.5h; | 82% |
Nitroethane
1,4,5,8-tetra(amino)naphthalene
2,7-dimethylpyrimido[4,5,6-gh]perimidine
Conditions | Yield |
---|---|
With polyphosphoric acid at 110℃; for 3h; | 78% |
1-nitro-1-phenylmethane
1,4,5,8-tetra(amino)naphthalene
2,7-diphenylpyrimido[4,5,6-gh]perimidine
Conditions | Yield |
---|---|
With polyphosphoric acid at 150℃; for 8h; | 63% |
Conditions | Yield |
---|---|
With polyphosphoric acid at 100℃; for 14h; | 56% |
1,4,5,8-tetra(amino)naphthalene
naphtho<1,8-cd:5,4-c'd'>bis<1,2,6>thia(SIV)diazine
Conditions | Yield |
---|---|
With 1-piperidinosulfenyl chloride In diethyl ether at -20℃; | 25% |
1,4,5,8-tetra(amino)naphthalene
dimethyl sulfate
1,4,5,8-Tetrakis(dimethylamino)naphthalene
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 25 - 60℃; | 14% |
1,4,5,8-tetra(amino)naphthalene
A
tris(dimethylamino)iminophosphorane hydrobromide
B
1,6-bis(dimethylamino)-2,5,7,10-tetraazo-1,6λ5-diphosphapyrene
Conditions | Yield |
---|---|
Stage #1: 1,4,5,8-tetra(amino)naphthalene; tris(dimethylamino)-bromophosphonium bromide With triethylamine In chlorobenzene at 20℃; for 72h; Inert atmosphere; Stage #2: With sodium hexamethyldisilazane In chlorobenzene; toluene for 24h; Inert atmosphere; | A n/a B 2.14% |