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| CAS No.: | 2389-48-2 | ||
|---|---|---|---|
| Name: | N-Boc-L-lysine methyl ester hydrochloride | ||
| Molecular Structure: | |||
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| Formula: | C12H24 N2 O4 . Cl H | ||
| Molecular Weight: | 296.794 | ||
| Synonyms: | L-Lysine,N6-[(1,1-dimethylethoxy)carbonyl]-, methyl ester, monohydrochloride (9CI);Lysine, N6-carboxy-, N-tert-butyl methyl ester, monohydrochloride, L-(6CI,7CI,8CI); Methyl (2S)-2-amino-6-[(tert-butoxycarbonyl)amino]hexanoatehydrochloride; Ne-BOC-L-lysinemethyl ester hydrochloride; Ne-tert-Butoxycarbonyllysine methyl ester hydrochloride | ||
| Density: | g/cm3 | ||
| Melting Point: | 158-159 °C(Solv: methanol (67-56-1); ethyl ether (60-29-7)) | ||
| Boiling Point: | 364.6°Cat760mmHg | ||
| Flash Point: | 174.3°C | ||
| Safety: |
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| PSA: | 90.65000 | ||
| LogP: | 3.07490 | ||
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- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 2937-50-0
Allyl chloroformate
- 140174-71-6
N-α-Alloc-N-ε-Boc-L-lysine methyl ester
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0 - 20℃; for 16h; | 100% |
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 215161-79-8
N,N'-bis(N-(carboxymethyl))-N,N'-bis(N-(2-(4-fluorophenyl)ethyl)carboxamidomethyl)benzene-1,3-dicarboxamide
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In N,N-dimethyl-formamide at 25℃; for 12h; Condensation; | 99% |
- 4285-42-1
N-phenyl-N-methylcarbamoyl chloride
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 1462366-90-0
methyl N6-(tert-butoxycarbonyl)-N2-(methyl(phenyl)carbamoyl)-L-lysinate
| Conditions | Yield |
|---|---|
| With triethylamine In acetonitrile for 15h; Reflux; | 99% |
| With dmap; triethylamine In 1,2-dimethoxyethane for 2h; Inert atmosphere; Reflux; | 93% |
- 3262-72-4
(S)-N-(tert-butoxycarbonyl)serine
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
| Conditions | Yield |
|---|---|
| With C12H6B2Br4O3 In 1,2-dichloro-ethane at 90℃; for 24h; Molecular sieve; chemoselective reaction; | 99% |
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 57-10-3
1-hexadecylcarboxylic acid
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 22h; Cooling with ice; | 98% |
| With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 22h; Inert atmosphere; | 57% |
- 3006-58-4, 13030-01-8, 42890-10-8, 42973-23-9, 77059-32-6, 121785-09-9, 7474-40-0
2-carbobenzyloxyamino-2-deoxy-D-glucopyranose
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 315229-51-7
(S)-2-((2S,3R,4S,5R)-2-Benzyloxycarbonylamino-3,4,5,6-tetrahydroxy-hexylamino)-6-tert-butoxycarbonylamino-hexanoic acid methyl ester
| Conditions | Yield |
|---|---|
| With sodium cyanoborohydride In methanol for 8h; Condensation; reduction; Heating; | 97% |
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 171813-89-1
(2S)-2-acetamido-3-(4-allyloxyphenyl)propanoic acid
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Sealed tube; Inert atmosphere; | 94% |
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 14h; Inert atmosphere; Sealed tube; | 94% |
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 95494-51-2
4-(4-oxo-3,4-dihydro-quinazolin-2-yl)-butyric acid
- 1310488-10-8
methyl 6-(tert-butoxycarbonylamino)-2-(4-(4-oxo-3,4-dihydroquinazolin-2-yl)butanamido)hexanoate
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; N,N-dimethyl-formamide | 93% |
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 48.5h; | 93% |
- 2483-46-7
Boc-Lys(Boc)-OH
- 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride
- 1350811-87-8
(S)-methyl 2-((S)-2,6-bis((tert-butoxycarbonyl)amino)hexanamido)-6-((tert-butoxycarbonyl)amino)hexanoate
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 92% |
| With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Cooling with ice; | 78.1% |
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Chemistry
Formula Weight: 296.79
Synonyms: H-LYS(BOC)-OME HCL;H-LYS(BOC)-OME HYDROCHLORIDE; N-EPSILON-BOC-L-LYSINE METHYL ESTER HYDROCHLORIDE; N-epsilon-t-Butyloxycarbonyl-L-lysine methyl ester hydrochloride; N-EPSILON-T-BOC-L-LYSINE METHYL ESTER HYDROCHLORIDE
Melting Point of H-Lys(Boc)-OMe·HCl (2389-48-2): 155-165 °C
Flash Point of H-Lys(Boc)-OMe·HCl (2389-48-2): 174.3 °C
Boiling Point: 364.6 °C at 760 mmHg
Vapour Pressure: 1.67E-05 mmHg at 25°C
storage temp. : 2-8°C
Appearance: H-Lys(Boc)-OMe·HCl (2389-48-2) is a white powder
Safety Profile
Standards and Recommendations
Specific Rotation: +16±2°(c=1inMeOH)