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| CAS No.: | 24958-42-7 |
|---|---|
| Name: | 2-Bromo-4-methoxy-5-benzyloxybenzoic acid |
| Article Data: | 3 |
| Molecular Structure: | |
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| Formula: | C15H13BrO4 |
| Molecular Weight: | 337.17 |
| Synonyms: | Benzoicacid, 5-(benzyloxy)-2-bromo-4-methoxy- (8CI);2-Bromo-5-benzyloxy-4-methoxybenzoic acid;5-(Benzyloxy)-2-bromo-4-methoxybenzoicacid; |
| Density: | 1.486 g/cm3 |
| Melting Point: | 193.0 to 197.0 °C |
| Boiling Point: | 445.442 ºC at 760 mmHg |
| Flash Point: | 223.196 ºC |
| PSA: | 55.76000 |
| LogP: | 3.73490 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 6451-86-1
5-benzyloxy-2-bromo-4-methoxybenzaldehyde
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
| Conditions | Yield |
|---|---|
| With potassium permanganate In methanol; water at 50 - 55℃; | 70% |
| Stage #1: 5-benzyloxy-2-bromo-4-methoxybenzaldehyde With hydrogenchloride; potassium permanganate In acetone Stage #2: With potassium hydroxide In acetone |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
- 38961-21-6
[2-(4-benzyloxy-phenyl)-ethyl]methylamine
- 24958-43-8
5-benzyloxy-N-[2-(4-benzyloxy-phenyl)-ethyl]-2-bromo-4-methoxy-N-methylbenzamide
| Conditions | Yield |
|---|---|
| With phenylboronic acid In toluene at 110℃; for 30h; | 93% |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
- 108-46-3
recorcinol
| Conditions | Yield |
|---|---|
| Stage #1: 2-bromo-4-methoxy-5-benzyloxy-benzoic acid; recorcinol With sodium hydroxide In water at 120℃; for 0.75h; Stage #2: With copper(II) sulfate In water for 0.25h; Reflux; | 52% |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
- 27240-64-8
5-Benzyloxy-2-bromo-4-methoxybenzoylchlorid
| Conditions | Yield |
|---|---|
| With thionyl chloride; N,N-dimethyl-formamide at 20℃; for 12h; Chlorination; | |
| With thionyl chloride; N,N-dimethyl-formamide In dichloromethane Substitution; | |
| With thionyl chloride In chloroform for 3h; Heating / reflux; | |
| With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 30 - 35℃; for 0.5h; | |
| With thionyl chloride; N,N-dimethyl-formamide In toluene at 68℃; for 2h; |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
- 206002-18-8
N-[(diphenylphosphinyl)methyl]-N-[(4-methoxyphenyl)methyl]-5-(benzyloxy)-2-bromo-4-methoxybenzamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: SOCl2; DMF / CH2Cl2 View Scheme | |
| Multi-step reaction with 2 steps 1: thionyl chloride; dimethylformamide / 12 h / 20 °C 2: Et3N / CH2Cl2 / 2 h / 0 - 20 °C View Scheme |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1.1: SOCl2; DMF / CH2Cl2 3.1: KHMDS / toluene; tetrahydrofuran / 2.5 h / -78 - 20 °C 3.2: 67 percent / NaOH; H2O / toluene; tetrahydrofuran / 3 h / Heating View Scheme |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1.1: thionyl chloride; dimethylformamide / 12 h / 20 °C 2.1: Et3N / CH2Cl2 / 2 h / 0 - 20 °C 3.1: KHMDS / toluene; tetrahydrofuran / 3.5 h / -78 - -30 °C 3.2: 81 percent / toluene; tetrahydrofuran / 0.5 h / -30 - 20 °C View Scheme |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
- 2592-95-2
benzotriazol-1-ol
- 873195-14-3
5-benzyloxy-2-bromo-4-methoxy benzoic acid benzotriazole-1-yl ester
| Conditions | Yield |
|---|---|
| Stage #1: 2-bromo-4-methoxy-5-benzyloxy-benzoic acid; benzotriazol-1-ol In dichloromethane at 25 - 35℃; for 0.25h; Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at 25 - 45℃; for 3 - 6h; Product distribution / selectivity; |
- 942-24-5
3-methoxycarbonylindole
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
| Conditions | Yield |
|---|---|
| With copper(l) iodide; potassium carbonate In N,N-dimethyl-formamide at 90℃; for 16h; Inert atmosphere; | |
| With copper(l) iodide; potassium carbonate In N,N-dimethyl-formamide at 90℃; for 16h; Inert atmosphere; |
- 24958-42-7
2-bromo-4-methoxy-5-benzyloxy-benzoic acid
| Conditions | Yield |
|---|---|
| With copper(l) iodide; potassium carbonate In N,N-dimethyl-formamide at 80℃; for 16h; Inert atmosphere; | |
| With copper(l) iodide; potassium carbonate In N,N-dimethyl-formamide at 80℃; for 16h; Inert atmosphere; |
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Chemistry
Product Name: Benzoic acid,2-bromo-4-methoxy-5-(phenylmethoxy)-
Synonyms of Benzoic acid,2-bromo-4-methoxy-5-(phenylmethoxy)- (CAS NO.24958-42-7): 3-Bromo-4-methoxy-5-benzyloxybenzoic acid ; 5-Benzyloxy-2-bromo-4-methoxy-benzoic acid ; 2-Bromo-5-benzyloxy-4-methoxybenzoic acid ; 2-Bromo-4-methoxy-5-(Benzyloxy)benzoic acid ; 2-Bromo-4-methoxy-5-(phenylmethoxy)benzoic acid ; 5-Benzyloxy-2-Bromo-4-Methoxyb ; 2-Brono-5-benzyloxy-4-methoxybenzoic acid ; 5-Benzyl-2-bromo-4-methoxylbenzoic acid
CAS NO: 24958-42-7
Molecular Formula of Benzoic acid,2-bromo-4-methoxy-5-(phenylmethoxy)- (CAS NO.24958-42-7): C15H13BrO4
Molecular Weight: 337.1653
Molecular Structure:
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ProductCategories: Multisubstituted Benzene ; Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts ; API intermediates
Polar Surface Area: 55.76 Å2
Index of Refraction: 1.611
Molar Refractivity: 78.718 cm3
Molar Volume: 226.854 cm3
Surface Tension: 50.715 dyne/cm
Density of Benzoic acid,2-bromo-4-methoxy-5-(phenylmethoxy)- (CAS NO.24958-42-7): 1.486 g/cm3
Flash Point: 223.196 °C
Enthalpy of Vaporization: 74.134 kJ/mol
Boiling Point: 445.442 °C at 760 mmHg
Vapour Pressure: 0 mmHg at 25°C