Products Categories
Basic Information
| CAS No.: | 2523-56-0 |
|---|---|
| Name: | cis-4-Methylcyclohexylamine. |
| Molecular Structure: | |
|
|
|
| Formula: | C7H15 N |
| Molecular Weight: | 113.203 |
| Synonyms: | Cyclohexylamine,4-methyl-, cis- (8CI); 4-cis-Methylcyclohexanamine;4-cis-Methylcyclohexylamine; cis-1-Amino-4-methylcyclohexane; cis-4-Methyl-1-cyclohexanamine;cis-4-Methylcyclohexylamine |
| Density: | 0.844 |
| Melting Point: | -8.5°C (estimate) |
| Boiling Point: | 154℃ |
| Flash Point: | 27℃ |
| PSA: | 26.02000 |
| LogP: | 2.22410 |
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Synthetic route
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| With aminosulfonic acid; sodium hydroxide In acetonitrile at 20 - 25℃; for 16h; Inert atmosphere; | 90% |
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| With aminosulfonic acid; potassium hydroxide In acetonitrile at 20 - 25℃; for 16h; Inert atmosphere; | 86.5% |
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| With aminosulfonic acid; sodium hydroxide In tetrahydrofuran at 20 - 25℃; for 16h; Inert atmosphere; Large scale; | 85% |
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| With aminosulfonic acid; lithium hydroxide In tetrahydrofuran at 20 - 25℃; for 16h; Inert atmosphere; | 81% |
- 106-49-0
p-toluidine
A
- 2523-55-9
trans-4-methylcyclohexanamine
B
- 2523-56-0
cis-4-methylcyclohexanamine
C
- 84518-71-8, 109667-09-6
4,4'-dimethyldicyclohexylamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen In tetrahydrofuran at 110℃; under 75007.5 Torr; for 3h; Kinetics; Reagent/catalyst; Temperature; Autoclave; | A 63.6% B 30.2% C n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; hydrogen; acetic acid; platinum at 25℃; under 2280 Torr; | |
| With hydrogen; silica gel; rhodium In 2,2,4-trimethylpentane at 49.85℃; Product distribution; Further Variations:; Catalysts; | |
| With hydrogen In 1,4-dioxane at 100℃; under 15001.5 Torr; for 3.33333h; Autoclave; | A n/a B n/a |
- 77287-34-4, 77287-35-5, 60100-09-6
formamide
- 589-92-4
1-methylcyclohexan-4-one
A
- 2523-55-9
trans-4-methylcyclohexanamine
B
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| With formic acid anschliessendes Erhitzen mit wss.HCl; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; acetic acid; platinum at 70 - 80℃; under 2280 Torr; anschliessend man verseift durch Erhitzen mit konz. Salzsaeure auf 130-140grad; |
- 34866-36-9
trans-4-methylcyclohexyl p-toluenesulfonate
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| (i) NaN3, (ii) H2, Pd-C, EtOH; Multistep reaction; | |
| With ammonia | |
| (i) NaN3, (ii) LiAlH4; Multistep reaction; |
- 589-92-4
1-methylcyclohexan-4-one
A
- 2523-55-9
trans-4-methylcyclohexanamine
B
- 2523-56-0
cis-4-methylcyclohexanamine
Conditions
| Conditions | Yield |
|---|---|
| Yield given. Multistep reaction. Yields of byproduct given; | |
| With decane; (S)-1-phenyl-ethylamine; Chromobacterium violaceum amine transaminase A W60 C In tert-butyl methyl ether at 37℃; pH=8.2; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
| With decane; (S)-1-phenyl-ethylamine; Vibrio fluvialis amine transaminase A In tert-butyl methyl ether at 37℃; pH=8.2; Catalytic behavior; Reagent/catalyst; Solvent; Enzymatic reaction; stereoselective reaction; | A n/a B n/a |
