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26555-40-8

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Basic Information
CAS No.: 26555-40-8
Name: METHOXYCARBONYLSULFENYL CHLORIDE
Article Data: 12
Molecular Structure:
Molecular Structure of 26555-40-8 (METHOXYCARBONYLSULFENYL CHLORIDE)
Formula: C2H3 Cl O2 S
Molecular Weight: 126.564
Synonyms: Carbonicacid, thio-, anhydrosulfide with thiohypochlorous acid, methyl ester (8CI);Carbonothioic acid, anhydrosulfide with thiohypochlorous acid, O-methyl ester(9CI); Thiohypochlorous acid, anhydrosulfide with O-methyl thiocarbonate (8CI);(Chlorothio)(methoxy)oxomethane; Carbomethoxysulfenyl chloride;Methoxycarbonylsulfenyl chloride; Methyl (chlorosulfenyl)formate
Density: 1.4g/cm3
Boiling Point: 133.5°Cat760mmHg
Flash Point: 34.5°C
Appearance: CLEAR BRIGHT YELLOW LIQUID
Hazard Symbols:
Risk Codes: 10-34
Safety:
Hazard Codes C
Risk Statements 10-34
Safety Statements 26-36/37/39-45
RIDADR UN 2920 8/PG 2
WGK Germany 3
F 10-21
HazardClass 8
PackingGroup II
PSA: 51.60000
LogP: 1.63980
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Synthetic route
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Conditions
ConditionsYield
In diethyl ether for 16h; Heating;88%
In diethyl ether
In tetrahydrofuran at 0℃; for 0.25h;
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Conditions
ConditionsYield
equimolar amts. of educts;20%
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Conditions
ConditionsYield
With chlorine
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bis(methoxycarbonyl)sulfide

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Conditions
ConditionsYield
With sulfuryl dichloride; chlorine
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Conditions
ConditionsYield
In chloroform-d1 at 62℃;
In chloroform-d1 at 62℃; Rate constant;
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chloro(chlorosulfanyl)methanone

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Conditions
ConditionsYield
In methanol
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chloro(chlorosulfanyl)methanone

A

2-chloro-4-(1-cyano-1-methylethylamino)-6-(N-ethyl-N-((methoxycarbonyl)thio))-1,3,5-triazine

2-chloro-4-(1-cyano-1-methylethylamino)-6-(N-ethyl-N-((methoxycarbonyl)thio))-1,3,5-triazine

B

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Methoxycarbonylsulfenyl chloride

Conditions
ConditionsYield
In methanol
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Methoxycarbonylsulfenyl chloride

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3-mercaptopropionic acid

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Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; Inert atmosphere;100%
With N,O-bis-(trimethylsilyl)-acetamide 1.) CH2Cl2, 1.5 h, 2.) CH2Cl2, 25 deg C, 2 h; Yield given. Multistep reaction;

(4R)-1-{[6-(4-fluorophenoxy)pyridin-3-yl]methyl}-4-mercaptopyrrolidin-2-one dihydrochloride

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Methoxycarbonylsulfenyl chloride

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2-(4-fluorophenoxy)-5-(((4R)-4-((methoxycarbonyl)dithio)-2-oxo-1-pyrrolidinyl)methyl)pyridine

Conditions
ConditionsYield
In methanol at 20℃; for 0.5h;100%
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Methoxycarbonylsulfenyl chloride

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4-mercaptophenylacetic acid

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Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; Inert atmosphere;100%
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