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27143-07-3

Basic Information
CAS No.: 27143-07-3
Name: Acetic acid, 2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene], ethyl ester
Article Data: 12
Molecular Structure:
Molecular Structure of 27143-07-3 (Acetic acid, 2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene], ethyl ester)
Formula: C11H13ClN2O3
Molecular Weight: 256.689
Synonyms: Chloro[(4-methoxyphenyl)hydrazono]acetic acid ethyl ester;
EINECS: 608-053-7
Density: 1.231 g/cm3
Melting Point: 94 ºC
Boiling Point: 348.955 ºC at 760 mmHg
Flash Point: 164.842 ºC
PSA: 59.92000
LogP: 2.29550
Synthetic route
104-94-9

4-methoxy-aniline

609-15-4

ethyl 2-chloro-3-oxo-butyrate

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

Conditions
ConditionsYield
Stage #1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite In water at -10 - -5℃; for 0.5h;
Stage #2: ethyl 2-chloro-3-oxo-butyrate With sodium acetate In water at -10 - -5℃; for 2h;
89%
Stage #1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite In ethanol; water at 0 - 5℃; for 0.5h;
Stage #2: ethyl 2-chloro-3-oxo-butyrate With sodium acetate In ethanol; water at 0 - 25℃;
85%
Stage #1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h;
Stage #2: ethyl 2-chloro-3-oxo-butyrate With sodium acetate In ethanol; water at -5 - 20℃; for 4h;
73.6%
104-94-9

4-methoxy-aniline

105-39-5

chloroacetic acid ethyl ester

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

Conditions
ConditionsYield
With hydrogenchloride; sodium acetate; sodium nitrite 1.) water; 2.) water, ethanol, 0 - 5 deg C, 3 h -> overnight; Multistep reaction;
638-07-3

ethyl (2-chloroaceto)acetate

104-94-9

4-methoxy-aniline

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

Conditions
ConditionsYield
Stage #1: 4-methoxy-aniline With hydrogenchloride In water at 40℃; for 0.416667h;
Stage #2: With sodium nitrite In water at -2℃; for 0.583333h;
Stage #3: ethyl (2-chloroaceto)acetate With aminosulfonic acid; sodium acetate more than 3 stages;

C11H10N2O4

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

C22H22N4O7

Conditions
ConditionsYield
With triethylamine In ethyl acetate at 70℃;95%

(2E,2'E)-1,4-bis[(2-(3-(dimethylamino)-1-oxoprop-2-en-1-yl)benzofuran-5-yl)methyl]piperazine

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

1,4-bis[((2-(3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrazole-4-yl)carbonyl)benzofuran-5-yl)methyl]piperazine

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane for 6h; Reflux; regioselective reaction;95%
503615-03-0

3-(morpholin-4-yl)-1-(4-nitrophenyl)-5,6-dihydropyridin-2(1H)-one

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

4,5,6,7-tetrahydro-1-(4-methoxyphenyl)-6-(4-nitrophenyl)-7-oxo- 1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
Stage #1: 3-(morpholin-4-yl)-1-(4-nitrophenyl)-5,6-dihydropyridin-2(1H)-one; ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate With triethylamine; potassium iodide In ethyl acetate for 4.5h; Reflux;
Stage #2: With hydrogenchloride In water; ethyl acetate at 5 - 20℃; for 4h;
94.6%
43052-77-3

(3,4-dihydro-6,7-dimethoxyisoquinolin-1-yl)acetonitrile

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

8,9-Dimethoxy-2-[(4-methoxy-phenyl)-hydrazono]-3-oxo-2,3,5,6-tetrahydro-pyrrolo[2,1-a]isoquinoline-1-carbonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol for 1h; Ambient temperature;90%
27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

60-10-6

1,5-diphenyl-3-mercaptoformazan

2-ethoxy-N′-(4-methoxyphenyl)-2-oxoacetohydrazonic-N′,2-diphenyldiazenecarbohydrazonic thioanhydride

Conditions
ConditionsYield
With sodium ethanolate In ethanol for 2h;90%
545445-44-1

5,6‑dihydro‑3‑(4‑morpholinyl)‑1‑[4‑(2‑oxo‑1‑piperidinyl)phenyl]‑2(1H)‑pyridone

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

503614-91-3

1-(4-methoxy-phenyl)-7-oxo-6-[4-(2-oxo-piperidin-1-yl)-phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With triethylamine; potassium iodide In ethyl acetate for 24h; Reflux;89.9%
With potassium carbonate; carbonic acid dimethyl ester at 82℃; for 0.5h; Temperature; Reagent/catalyst;80.33%
With triethylamine In ethyl acetate; toluene at 85℃; for 7h;76%
With triethylamine; potassium iodide In ethyl acetate at 25 - 80℃; for 24h;54 mg
Stage #1: 5,6‑dihydro‑3‑(4‑morpholinyl)‑1‑[4‑(2‑oxo‑1‑piperidinyl)phenyl]‑2(1H)‑pyridone; ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate With triethylamine
Stage #2: With hydrogenchloride In water

2-(1-(10H-phenothiazin-2-yl)ethylidene)hydrazine-1-carbothioamide

27143-07-3

ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate

2-(2-(1-(10H-phenothiazin-2-yl)ethylidene)hydrazinyl)-5-(2-(4-methoxyphenyl)hydrazono)thiazol-4(5H)-one

Conditions
ConditionsYield
With triethylamine In ethanol at 110℃; for 0.25h; Microwave irradiation;88%
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503614-91-3
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  • Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

  • Casno:

    27143-07-3

    MSDS/COA Download

    Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 400.0-500.0

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  • ethyl (2Z)-2-chloro-2-[(4-methoxyphenyl)hydraziny -lidene]acetate

  • Casno:

    27143-07-3

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    ethyl (2Z)-2-chloro-2-[(4-methoxyphenyl)hydraziny -lidene]acetate

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    ETHYL(2Z)-2-CHLORO-2-[(4-METHOXYPHENYL)HYDRAZINY-LIDENE]ACETATE (27143-07-3) Information The product is Apixaban intermediate. Quality Advanced technology Supper qual

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  • Apixaban intermediate 27143-07-3

  • Casno:

    27143-07-3

    Apixaban intermediate 27143-07-3

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

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  • Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

  • Casno:

    27143-07-3

    Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

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  •  Hangzhou Keyingchem Co.,Ltd

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    Business Type:Lab/Research institutions

    Tel:+86-571-85378921

    Address:Jintong international Building, No.113,Huayuangang Street, Gong shu District, Hangzhou,Zhejiang, China.

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  • Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

  • Casno:

    27143-07-3

    Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    Name Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate Synonyms Chloro[(4-methoxyphenyl)hydrazono]acetic acid ethyl ester Molecular Structure

    Hangzhou Jinlan Pharm-Drugs Technology Co.,Ltd is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pudon

  •  Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

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    Business Type:Other

    Tel:+86-571-85829053

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  • ACETIC ACID, 2-CHLORO-2-[2-(4-METHOXYPHENYL)HYDRAZINYLIDENE], ETHYL ESTER

  • Casno:

    27143-07-3

    ACETIC ACID, 2-CHLORO-2-[2-(4-METHOXYPHENYL)HYDRAZINYLIDENE], ETHYL ESTER

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

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    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • Ethyl chloro[(4-methoxyphenyl)-hydrazono]acetate

  • Casno:

    27143-07-3

    Ethyl chloro[(4-methoxyphenyl)-hydrazono]acetate

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    1. made in GMP plant, commerially 2. usually have it in stock 3. can supply at large quantity 4. audit accepted. related documents are available to offer and audited by many clients, such as lupin, msn, dr reddy etc 5. chromatographic p

    Shanghai SE Pharm Co., Ltd was headquartered in Shanghai Pudong new District. Our advantages are project analysis & integration and resources intergration according to the markets.

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     China (Mainland)  |  Contact Details

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    Address:Room 301, Building 1, Wuxing Road 707#, Pudong New district, Shanghai

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  • Acetic acid, 2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene], ethyl ester

  • Casno:

    27143-07-3

    Acetic acid, 2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene], ethyl ester

    Min.Order: 4 Kilogram

    FOB Price:  USD $ 0.0-0.0

    A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

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  •  SHANGHAI T&W PHARMACEUTICAL CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-61551611

    Address:601, No. 1, 2277 Nong, Zu Chongzhi Road, Zhangjiang Hightech. Park, Pudong

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Specification

The Ethyl chloro[(4-methoxyphenyl)hydrazono]acetate, with its CAS registry number 27143-07-3, has other names as Chloro[(4-methoxyphenyl)hydrazono]acetic acid ethyl ester.

The characteristics of this chemical are as below: (1)ACD/LogP: 2.34; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 3; (4)ACD/LogD (pH 7.4): 3; (5)ACD/BCF (pH 5.5): 151; (6)ACD/BCF (pH 7.4): 151; (7)ACD/KOC (pH 5.5): 1261; (8)ACD/KOC (pH 7.4): 1261; (9)#H bond acceptors: 5; (10)#H bond donors: 1; (11)#Freely Rotating Bonds: 6; (12)Polar Surface Area: 59.92; (13)Index of Refraction: 1.533; (14)Molar Refractivity: 64.659 cm3; (15)Molar Volume: 208.488 cm3; (16)Polarizability: 25.633 ×10-24 cm3; (17)Surface Tension: 39.176 dyne/cm; (18)Density: 1.231 g/cm3; (19)Flash Point: 164.842 °C; (20)Enthalpy of Vaporization: 59.339 kJ/mol; (21)Boiling Point: 348.955 °C at 760 mmHg. 

Additionally, you could convert the following datas into the molecular structure:
(1)SMILES:COc1ccc(N\N=C(\Cl)C(=O)OCC)cc1
(2)InChI:InChI=1/C11H13ClN2O3/c1-3-17-11(15)10(12)14-13-8-4-6-9(16-2)7-5-8/h4-7,13H,3H2,1-2H3
(3)InChIKey:ATNPZEGMKLGIFA-UHFFFAOYAJ