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28343-22-8

Basic Information
CAS No.: 28343-22-8
Name: Phenol,4-ethenyl-2,6-dimethoxy-
Molecular Structure:
Molecular Structure of 28343-22-8 (Phenol,4-ethenyl-2,6-dimethoxy-)
Formula: C10H12 O3
Molecular Weight: 180.2
Synonyms: Phenol,2,6-dimethoxy-4-vinyl- (8CI); 2,6-Dimethoxy-4-ethenylphenol;2,6-Dimethoxy-4-vinylphenol; 3,5-Dimethoxy-4-hydroxystyrene;4-Vinyl-2,6-dimethoxyphenol; 4-Vinylsyringol; Canolol; Syringlyethene;Vinylsyringol
EINECS:
Density: 1.113g/cm3
Melting Point:
Boiling Point: 285.4°Cat760mmHg
Flash Point: 126.4°C
Solubility:
Appearance:
Hazard Symbols:
Risk Codes:
Safety:
Transport Information:
PSA: 38.69000
LogP: 2.05240
Synthetic route
530-59-6

sinapinic acid

28343-22-8

canolol

Conditions
ConditionsYield
With Cocos nucifera juice at 20℃; for 48h; Inert atmosphere;94%
With aluminum oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinone In methanol for 0.25h; microwave irradiation;84%
With 1,10-Phenanthroline; copper hydroxide In 1-methyl-pyrrolidin-2-one at 130℃; for 1.1h; Inert atmosphere; Green chemistry;31%
33900-62-8

1-(4-Hydroxy-3,5-dimethoxyphenyl)ethanol

28343-22-8

canolol

Conditions
ConditionsYield
With MoO2Cl2(DMSO)2; dimethyl sulfoxide for 0.166667h; Microwave irradiation;90%
With MoO2(2+)*C2H6OS*2Cl(1-) In dimethyl sulfoxide for 0.166667h; Microwave irradiation;90%
With 1-hexyl-3-methyl-1-imidazolium bromide at 150℃; for 0.25h; Microwave irradiation;
141-82-2

malonic acid

134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
With pyridine; acetic acid at 130℃; for 0.116667h; microwave irradiation;67%
With piperidine In 1-methyl-pyrrolidin-2-one for 3h; Reflux;67.5%
With piperidine In toluene at 115℃; Knoevenagel-Doebner-Stobbe Reaction;47%
134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
With Methyltriphenylphosphonium bromide; sodium hexamethyldisilazane In tetrahydrofuran for 5.5h; Cooling;59%
1779-49-3

Methyltriphenylphosphonium bromide

134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With sodium hexamethyldisilazane In tetrahydrofuran for 1.5h; Cooling;
Stage #2: syringic aldehyde In tetrahydrofuran for 4h;
18%
forest plant material

forest plant material

A

91-10-1

1,3-dimethoxy-2-hydroxy-benzene

B

6638-05-7

2,6-dimethoxy-4-methylphenol

C

14059-92-8

4-ethylsyringol

D

28343-22-8

canolol

Conditions
ConditionsYield
With air Oxidation; Formation of xenobiotics; Further byproducts given;
1252786-17-6

C4H11N*C11H12O5

A

1252786-39-2

C4H11N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 51 %Spectr.
B 5 %Spectr.

C4H11NO*C11H12O5

A

C4H11NO*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 50 %Spectr.
B 5 %Spectr.
1252786-19-8

C2H7NO*C11H12O5

A

1252786-41-6

C2H7NO*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 15 %Spectr.
B 7 %Spectr.
1252786-21-2

C5H11N*C11H12O5

A

1252786-43-8

C5H11N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 67 %Spectr.
B 4 %Spectr.
1252786-20-1

C8H11N*C11H12O5

A

1252786-42-7

C8H11N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 46 %Spectr.
B 4 %Spectr.
1252786-22-3

C6H13N*C11H12O5

A

1252786-44-9

C6H13N*C11H12O5

B

28343-22-8

canolol

Conditions
ConditionsYield
In acetonitrile for 24h; UV-irradiation;A 46 %Spectr.
B 4 %Spectr.
2065-66-9

methyl-triphenylphosphonium iodide

134-96-3

syringic aldehyde

28343-22-8

canolol

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran Wittig Olefination;
With potassium tert-butylate In tetrahydrofuran Wittig Olefination;
65109-39-9

4-(2-(2,6-dimethoxyphenoxy)-1-hydroxyethyl)-2,6-dimethoxyphenol

A

91-10-1

1,3-dimethoxy-2-hydroxy-benzene

B

2478-38-8

1-(4-hydroxy-3,5-dimethoxy-phenyl)-ethanone

C

612-69-1

3,5,3',5'-tetramethoxybiphenyl-4,4'-diol

D

537-35-9

1,2-Disyringylethane

E

28343-22-8

canolol

F

20824-45-7

4-hydroxy-3,5-dimethoxyphenethyl alcohol

G

136273-00-2

1,2-Disyringylethene

H

101788-35-6

3,5,3',5'-tetramethoxy-bibenzyl-4,α,4'-triol

I

C18H22O6

J

C18H20O6

K

C27H32O8

L

134-96-3

syringic aldehyde

Conditions
ConditionsYield
With sodium hydroxide at 170℃; for 1h;
28343-22-8

canolol

106-89-8

epichlorohydrin

2-((2,6-dimethoxy-4-vinylphenoxy)methyl)oxirane

Conditions
ConditionsYield
Stage #1: canolol; epichlorohydrin With N-benzyl-N,N,N-triethylammonium chloride at 100℃;
Stage #2: With sodium hydroxide In water at 30℃; for 1.5h;
90%
28343-22-8

canolol

C20H24O7

Conditions
ConditionsYield
With C21H33N2O5V; water; oxygen In acetonitrile at 60℃; for 16h;81%
28343-22-8

canolol

513-86-0, 52217-02-4

3-hydroxy-2-butanon

4-hydroxy-3-(4-hydroxy-3,5-dimethoxyphenyl)pent-3-en-2-one

Conditions
ConditionsYield
With monoaluminum phosphate In neat (no solvent) at 119.84℃;78%
28343-22-8

canolol

138526-69-9

3,4,5-trifluoro-1-bromobenzene

(E)-3,5-dimethoxy-4-hydroxy-3',4',5'-trifluorstilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Inert atmosphere;75.3%
20469-63-0

1-iodo-2,4-dimethoxybenzene

28343-22-8

canolol

(E)-4-hydroxy-2',3,4',5-tetramethoxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Inert atmosphere;72.8%
23030-43-5

2,5-dihydroxy-1-iodobenzene

28343-22-8

canolol

1449510-37-5

(E)-3,5-dimethoxy-4,2',5'-trihydroxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Heck Reaction; Inert atmosphere;65.3%
With triethanolamine; palladium diacetate at 100℃; for 24h; Inert atmosphere;65.3%
28343-22-8

canolol

malvidin 3-glucoside hydrochloride

7-hydroxy-2-(4-hydroxy-3,5-dimethoxyphenyl)-10-(3,5-dimethoxy-4-hydroxyphenyl)-pyrano[4,3,2-de]chromen-1-ylium-3-O-glucoside

Conditions
ConditionsYield
With hydrogenchloride In water; acetonitrile at 20 - 45℃; for 624h; pH=1.5;61%
25245-27-6

1-iodo-3,5-dimethoxybenzene

28343-22-8

canolol

(E)-4-hydroxy-3,3',5,5'-tetramethoxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; stereoselective reaction;57.9%

3,5-dimethoxy-4-fluoro-1-bromobenzene

28343-22-8

canolol

1394048-10-2

(E)-4'-fluoro-4-hydroxy-3,3',5,5'-tetramethoxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; stereoselective reaction;55.4%
28343-22-8

canolol

64339-43-1

5-iodoresorcinol

1394048-09-9

(E)-3,5-dimethoxy-3',4,5'-trihydroxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; stereoselective reaction;53.4%
With triethanolamine; palladium diacetate at 100℃; for 24h; Heck Reaction; Inert atmosphere;
28343-22-8

canolol

108-98-5

thiophenol

2,6-dimethoxy-4-(2-phenylsulfanylethyl)phenol

Conditions
ConditionsYield
With 1-hexyl-3-methyl-1-imidazolium bromide at 40℃; for 2h; regioselective reaction;51%
28343-22-8

canolol

108530-10-5

2-oxo-2H-benzopyran-7-yl trifluoromethanesulfonate

7-[(E)-2-(4-hydroxy-3,5-dimethoxyphenyl)ethenyl]-2H-chromen-2-one

Conditions
ConditionsYield
With triethanolamine; palladium diacetate for 0.5h; Heck Reaction; Reflux; Microwave irradiation;51%
25245-35-6

1-iodo-2,4-dimethoxybenzene

28343-22-8

canolol

1394048-11-3

(E)-4-hydroxy-2',3,5,5'-tetramethoxystilbene

Conditions
ConditionsYield
With triethanolamine; palladium diacetate at 100℃; for 24h; Mizoroki-Heck reaction; Inert atmosphere; stereoselective reaction;49%
28343-22-8

canolol

3-bromo-4-methyl-7-(octyloxy)-2H-chromen-2-one

3-[(E)-2-(4-hydroxy-3,5-dimethoxyphenyl)ethenyl]-4-methyl-7-(octyloxy)-2H-chromen-2-one

Conditions
ConditionsYield
With triethanolamine; palladium diacetate for 0.5h; Heck Reaction; Reflux; Microwave irradiation;41%

(2E)-1-(4-bromophenyl)-3-(4-hydroxy-3-methoxyphenyl) prop-2-en-1-one

28343-22-8

canolol

(E)-1-(4-((E)-4-hydroxy-3,5-dimethoxystyryl)phenyl)-3-(4-hydroxy-3-methoxyphenyl)prop-2-en-1-one

Conditions
ConditionsYield
With pyrrolidine; palladium diacetate; lithium chloride In N,N-dimethyl-formamide at 170℃; for 0.0666667h; Microwave irradiation;40%
28343-22-8

canolol

298-14-6

potassium hydrogencarbonate

530-59-6

trans-3,5-dimethoxy-4-hydroxycinnamic acid

Conditions
ConditionsYield
With phenolic acid decarboxylase from Pantoea sp. In aq. phosphate buffer; acetonitrile at 30℃; for 24h; pH=8.5; Reagent/catalyst; Sealed tube; Enzymatic reaction;
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    Address:hebei

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  • Phenol, 4-ethenyl-2,6-dimethoxy-

  • Casno:

    28343-22-8

    Phenol, 4-ethenyl-2,6-dimethoxy-

    Min.Order: 1 Gram

    FOB Price:  USD $ 1.0-1.0/Gram

    HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

    Hubei Ipure biotech Co., Ltd. is Established in 2011,which is located in Wuhan, Hubei Province where is the largest city in central China. The company is a diversified product pr

  • HuBei Ipure Biotech CO.,ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18062427325

    Address:NO 18. 81F street Future city ,Hongshan district ,WuHan city ,Hubei province ,China

       Inquiry Now

  • 2,6-dimethoxy-4-vinylphenol

  • Casno:

    28343-22-8

    2,6-dimethoxy-4-vinylphenol

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    2,6-dimethoxy-4-vinylphenol Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

  • Nanjing Raymon Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-025-52181296

    Address:Block B, No. 918, Shuanglong Avenue

       Inquiry Now

  • 4-VINYL-2,6-DIMETHOXY-PHENOL

  • Casno:

    28343-22-8

    4-VINYL-2,6-DIMETHOXY-PHENOL

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Angene supplies the compounds with the most competitive price and the best quality; specializes in custom synthesis & building blocks. Welcome the enquiries & orders around the world. Application:chemical research

    Angene is pledged to providing quality chemicals for use in research and development and commercial manufacturing. Angenes offers over 100,000 products including lab reagents, inte

  • Angene International Limited

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+852 8191 6999

    Address:CHURCHILL HOUSE 142-146 OLD STREET

       Inquiry Now

  • 28343-22-8

  • Casno:

    28343-22-8

    28343-22-8

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Supply top quality products with a reasonable price Application:api

    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

  • Hebei Ruishun Trade Co.,Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-311-68037669

    Address:WanDa commerce building ,yuhua district

       Inquiry Now

  • 4-VINYL-2,6-DIMETHOXY-PHENOL

  • Casno:

    28343-22-8

    4-VINYL-2,6-DIMETHOXY-PHENOL

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Our company provides the best service for our customers. Under the premise of ensuring quality and delivery date, give customers the best price. The company is more willing to meet our customers. If you want to visit our factories and warehouses, we

  • Sparrow Chemical Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-531-67865410

    Address:Jinan City,Shandong Province,China

       Inquiry Now

  • Total:22 Page 1 of 1 1

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