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Basic Information
| CAS No.: | 28910-91-0 |
|---|---|
| Name: | flualprazolam |
| Article Data: | 10 |
| Molecular Structure: | |
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|
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| Formula: | N/A |
| Molecular Weight: | 326.76 |
| Synonyms: | flualprazolam |
| Density: | 1.43±0.1 g/cm3(Predicted) |
| Boiling Point: | 509.8±60.0 °C(Predicted) |
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Synthetic route
- 1068-57-1
acetic acid hydrazide
- 59467-62-8
7-chloro-5-(2-fluorophenyl)-2-(N-nitrosomethylamino)-3H-1,4-benzodiazepine
- 28910-91-0
flualprazolam
Conditions
| Conditions | Yield |
|---|---|
| With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 120℃; for 1h; | 84% |
| With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 120℃; for 4h; | 280 mg |
- 1068-57-1
acetic acid hydrazide
- 2886-65-9
7-chloro-5-(2-fluorophenyl)-1,3-dihydro-1,4-benzodiazepin-2(2H)-one
- 28910-91-0
flualprazolam
Conditions
| Conditions | Yield |
|---|---|
| In butan-1-ol at 125℃; for 8h; Temperature; Solvent; | 81.2% |
- 1645-32-5
7-chloro-1,3-dihydro-5-(2-fluorophenyl)-2H-1,4-benzodiazepine-2-thione
- 28910-91-0
flualprazolam
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane; water; butan-1-ol |
- 2886-65-9
7-chloro-5-(2-fluorophenyl)-1,3-dihydro-1,4-benzodiazepin-2(2H)-one
- 28910-91-0
flualprazolam
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: titanium tetrachloride / tetrahydrofuran / 5.33 h / -5 - 45 °C / Inert atmosphere 2: acetic acid; sodium nitrite / water / 3.25 h / 3 - 25 °C 3: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 4 h / 120 °C View Scheme |
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