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Basic Information
CAS No.: 33100-15-1
Name: 2-(2-NITROPHENYL)ETHANAMINE
Molecular Structure:
Molecular Structure of 33100-15-1 (2-(2-NITROPHENYL)ETHANAMINE)
Formula: C8H10 N2 O2
Molecular Weight: 166.18
Synonyms: Phenethylamine,o-nitro- (6CI,8CI); 2-(2-Aminoethyl)nitrobenzene; b-(o-Nitrophenyl)ethylamine
Density: 1.206±0.06 g/cm3(Predicted)
Boiling Point: 147 °C(Press: 13 Torr)
PSA: 71.84000
LogP: 2.31950
Related products
Synthetic route
610-66-2

2-nitro-benzeneacetonitrile

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
Stage #1: 2-nitro-benzeneacetonitrile With dimethylsulfide borane complex In tetrahydrofuran at 0℃; for 8h; Heating / reflux;
Stage #2: With methanol for 1h; Heating / reflux;		100%
With borane-THF at 0 - 20℃; Inert atmosphere;82%
With dimethylsulfide borane complex In tetrahydrofuran at 0 - 70℃; for 8h; Inert atmosphere;82%
With borane-THF
2001-32-3

3-(2-nitrophenyl)propionic acid

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With hydrogen azide; chloroform; sulfuric acid
315663-43-5

N-(2-nitro-phenethyl)-acetamide

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With hydrogen bromide
64-04-0

phenethylamine

A

24954-67-4

2-(p-nitrophenyl)ethylamine

B

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With sulfuric acid; nitric acid
16793-89-8

(2-bromoethyl)-2-nitrobenzene

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
(i) aq. NaN3, DMSO, (ii) Ph3P, benzene, (iii) aq. HBr, AcOH; Multistep reaction;
Stage #1: (2-bromoethyl)-2-nitrobenzene With sodium azide In water; acetonitrile for 20h; Heating / reflux;
Stage #2: With triphenylphosphine In toluene at 20℃; for 16h;
Stage #3: With sodium hydroxide; hydrogen bromide; acetic acid more than 3 stages;
31142-60-6

2-(2-nitrophenyl)acetamide

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With borane In 1,4-dioxane
With borane
15121-84-3

2-nitro-benzeneethanol

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With dmap; trifluoromethylsulfonic anhydride; ammonia 1.) CH2Cl2, from -30 deg C to RT, 2.) THF, from -30 deg C to RT; Multistep reaction;
Multi-step reaction with 2 steps
1: aq. HBr
2: (i) aq. NaN3, DMSO, (ii) Ph3P, benzene, (iii) aq. HBr, AcOH
View Scheme
64-04-0

phenethylamine

HNO3+H2SO4

HNO3+H2SO4

A

24954-67-4

2-(p-nitrophenyl)ethylamine

B

33100-15-1

2-(2-aminoethyl)nitrobenzene

...Expand
7697-37-2

nitric acid

64-04-0

phenethylamine

A

24954-67-4

2-(p-nitrophenyl)ethylamine

B

33100-15-1

2-(2-aminoethyl)nitrobenzene

C

83304-13-6

2-(3-nitrophenyl)ethylamine

Conditions
ConditionsYield
at -10℃;
...Expand
2-nitro-hydrocinnamic acid bromoamide

2-nitro-hydrocinnamic acid bromoamide

33100-15-1

2-(2-aminoethyl)nitrobenzene

Conditions
ConditionsYield
With potassium hydroxide at 80 - 90℃;
Raw Materials
33100-26-4
16793-89-8
31142-60-6
2001-32-3
15121-84-3
877-95-2
31912-02-4
7697-37-2
Downstream Products
1500-42-1
48108-93-6
552-16-9
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