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Basic Information
CAS No.: 34432-92-3
Name: N-ethyl-N-[2-[1-(2-methylpropoxy)ethoxy]ethyl]-4-(phenylazo)aniline
Molecular Structure:
Molecular Structure of 34432-92-3 (N-ethyl-N-[2-[1-(2-methylpropoxy)ethoxy]ethyl]-4-(phenylazo)aniline)
Formula: C22H31 N3 O2
Molecular Weight: 369.507
Synonyms: Acetaldehyde,isobutyl 2-[N-ethyl-p-(phenylazo)anilino]ethyl acetal (8CI); Benzenamine,N-ethyl-N-[2-[1-(2-methylpropoxy)ethoxy]ethyl]-4-(phenylazo)- (9CI); C.I.111155; C.I. Solvent Yellow 124; Solvent Yellow 124
Density: 1.02g/cm3
Boiling Point: 488.9°Cat760mmHg
Flash Point: 249.5°C
Solubility: 30μg/L at 20℃
Hazard Symbols:
Risk Codes: 22
Safety:
Hazard Codes Xn
Risk Statements 22
PSA: 46.42000
LogP: 5.96350
Synthetic route

N-ethyl-N-(2-(1-isobutoxyethoxy)ethyl)aniline

100-34-5

benzene diazonium chloride

34432-92-3

C.I. Solvent Yellow 124

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 3 - 10℃; for 2.5h; pH=8.5 - 9.5; Reagent/catalyst; pH-value; Reflux;69.17%
62-53-3

aniline

34432-92-3

C.I. Solvent Yellow 124

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid; sodium nitrite / water / 1 h / 5 °C / pH <= 2
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 2.5 h / 3 - 10 °C / pH 8.5 - 9.5 / Reflux
View Scheme
92-50-2

2-( N-ethylanilino)ethanol

34432-92-3

C.I. Solvent Yellow 124

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium / tetrahydrofuran / 2 h / Reflux
2: tetrahydrofuran / 4.5 h / Reflux
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 2.5 h / 3 - 10 °C / pH 8.5 - 9.5 / Reflux
View Scheme
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