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3446-90-0

Basic Information
CAS No.: 3446-90-0
Name: 4-(Methylthio)benzyl Alcohol
Article Data: 43
Molecular Structure:
Molecular Structure of 3446-90-0 (4-(Methylthio)benzyl Alcohol)
Formula: C8H10 O S
Molecular Weight: 154.233
Synonyms: Benzylalcohol, p-(methylthio)- (7CI,8CI); 4-(Hydroxymethyl)phenyl methyl sulfide;4-(Methylmercapto)benzyl alcohol; 4-(Methylthio)benzenemethanol;4-(Methylthio)benzyl alcohol; 4-Methylsulfanylbenzyl alcohol;[4-(Methylsulfanyl)phenyl]methanol; p-(Methylthio)benzyl alcohol
Density: 1.15g/cm3
Melting Point: 38-42 ºC
Boiling Point: 108-109 ºC (0.4 mmHg)
Flash Point: 137.6°C
Solubility: Soluble in water.
Appearance: Colorless to light yellow liqui
Risk Codes: 36/37/38
Safety: S24/25
PSA: 45.53000
LogP: 1.90080
Synthetic route
3446-89-7

4-(Methylthio)benzaldehyde

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With hydrogen; phosphotungstic acid 44-hydrate; [Fe(C5H4P(i-Pr)2)2Rh(C8H12)]BF4 In water; isopropyl alcohol at 20℃; under 5171.62 Torr; for 16h;100%
With isopropyl alcohol; hydrotalcite at 81.84℃; for 3h; Kinetics; Further Variations:; Temperatures; Reagents;100%
Stage #1: 4-(Methylthio)benzaldehyde With chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II); phenylsilane at 80℃; for 0.666667h;
Stage #2: With tetrabutyl ammonium fluoride at 20℃; for 0.5h; Reagent/catalyst; Temperature; Time; Solvent; chemoselective reaction;
98%
102606-93-9

4-(methylthio)benzyl acetate

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With zirconocene dichloride; diisobutylaluminium hydride In tetrahydrofuran at -20℃; Inert atmosphere; regioselective reaction;99%
13205-48-6

4-(methylthio)benzoic acid

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 4h; Inert atmosphere;90.89%
With lithium aluminium tetrahydride; diethyl ether
With diborane In tetrahydrofuran at 0℃; for 1.5h;
21382-98-9

p-cyanophenyl methyl sulfide

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); water; hydrogen In 1,4-dioxane at 140℃; under 7500.75 Torr; for 69h; Autoclave;89%
3795-79-7

methyl 4-(methylthio)benzoate

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With HN(CH2CH2C3H3N2Mes)2Cl2; potassium tert-butylate; hydrogen; cobalt(II) chloride In tetrahydrofuran at 100℃; under 45004.5 Torr; for 16h; Autoclave; Glovebox;85%
With lithium aluminium tetrahydride
67-63-0

isopropyl alcohol

4-(methylthio)-benzyl-methoxymethyl ether

A

3446-90-0

4-(methylthio)benzyl alcohol

B

1-isopropoxymethyl-4-methylsulfanyl-benzene

Conditions
ConditionsYield
With carbon tetrabromide for 3h; Heating;A 85%
B 14%
67-63-0

isopropyl alcohol

4-(methylthio)-benzyl-methoxyethoxymethyl ether

A

3446-90-0

4-(methylthio)benzyl alcohol

B

1-isopropoxymethyl-4-methylsulfanyl-benzene

Conditions
ConditionsYield
With carbon tetrabromide for 3h; Heating;A 85%
B 11%

4-(methylthio)benzyl β-(trimethylsilyl)ethoxymethyl ether

3446-90-0

4-(methylthio)benzyl alcohol

Conditions
ConditionsYield
With carbon tetrabromide In isopropyl alcohol for 1.5h; Heating;85%
38185-19-2

4-(methylthio)benzyl bromide

A

3446-90-0

4-(methylthio)benzyl alcohol

B

51927-46-9

1-bromomethyl-4-methanesulfinylbenzene

C

3446-89-7

4-(Methylthio)benzaldehyde

Conditions
ConditionsYield
With dihydrogen peroxide at 70℃; for 1h;A n/a
B 52%
C n/a
3446-89-7

4-(Methylthio)benzaldehyde

766-97-2

4-n-methylphenylacetylene

A

3446-90-0

4-(methylthio)benzyl alcohol

B

1-(4-(methylthio)phenyl)-3-(p-tolyl)prop-2-yn-1-one

Conditions
ConditionsYield
With triethylamine; zinc(II) iodide In toluene at 80℃; for 12h; Schlenk technique; Inert atmosphere;A n/a
B 50%
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  • 4-(Methylthio)benzyl Alcohol

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    3446-90-0 Application:intermediate

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Business Type:Lab/Research institutions

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    Address:East Lake high tech Development Zone, Wuhan, 262, No.

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  • 3446-90-0

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    3446-90-0

    3446-90-0

    Min.Order: 0

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    Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

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    Business Type:Trading Company

    Tel:+8617316470195

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